环辛-4-烯-1-基乙酸酯合成路线 (共 8 条)
反应条件
pyridine in dichloromethane T=40°C; 20 h; Inert atmosphere;
参考文献
Blencowe, Anton; Qiao, Greg G.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5717 - 5725
反应条件
triethylamine in dichloromethane T=0 - 20°C; 12.5 h; Inert atmosphere;
参考文献
Zhang, Ke; Lackey, Melissa A.; Cui, Jun; Tew, Gregory N.
Journal of the American Chemical Society, 2011 , vol. 133, # 11 p. 4140 - 4148
反应条件
ruthenium hydroxide trichloride in dichloromethane T=180°C; 1 h; AutoclaveInert atmosphere;
参考文献
Khusnutdinov; Shchadneva; Khisamova; Dzhemilev
Russian Journal of Organic Chemistry, 2011 , vol. 47, # 2 p. 155 - 160
反应条件
sodium tetrahydroborate in dichloromethane
参考文献
Bloodworth, A.J.; Khan, Jamil A.; Loveitt, M.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 621 - 632
反应条件
1: 3-chloro-benzenecarboperoxoic acid / chloroform / 14 h / 20 °C 2: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere 3: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Blencowe, Anton; Qiao, Greg G.
Journal of the American Chemical Society, 2013 , vol. 135, # 15 p. 5717 - 5725
反应条件
1: lithium aluminium tetrahydride / tetrahydrofuran / 12 h / 0 - 20 °C / Inert atmosphere 2: triethylamine / dichloromethane / 12.5 h / 0 - 20 °C / Inert atmosphere View Scheme
参考文献
Zhang, Ke; Lackey, Melissa A.; Cui, Jun; Tew, Gregory N.
Journal of the American Chemical Society, 2011 , vol. 133, # 11 p. 4140 - 4148
参考文献
Cope; Wood
Journal of the American Chemical Society, 1957 , vol. 79, p. 3885,3888
Full Text Show Details
Cope; Johnson
Journal of the American Chemical Society, 1957 , vol. 79, p. 3889,3891
反应条件
sodium hydroxide; sodium tetrahydroborate; dihydrogen peroxide multistep reaction; (per)oxymercuriation of various cyclo-octadienes followed by reduction, influence of mercury(II) salt and reaction conditions; Product distribution;
参考文献
Bloodworth, A.J.; Khan, Jamil A.; Loveitt, M.E.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1981 , p. 621 - 632