N-乙氧羰基邻苯二甲酰亚胺合成路线 (共 86 条)
反应条件
1: With sodium carbonate in water 1 h; Inert atmosphere; 2: With hydrogenchloride in water 1 h;
参考文献
Muller, George W.; Konnecke, William E.; Smith, Alison M.; Khetani, Vikram D.
Organic Process Research and Development, 1999 , vol. 3, # 2 p. 139 - 140
反应条件
sodium carbonate 0.5 h;
参考文献
Ma, Yong Min; Hider, Robert C.
Bioorganic and Medicinal Chemistry, 2009 , vol. 17, # 23 p. 8093 - 8101
反应条件
1: [14C]-L-Tryptophan With sodium carbonate in water 2: N-ethoxycarbonylphthalimide in water T=20°C; 2 h;
参考文献
Suksiriworapong, Jiraphong; Sripha, Kittisak; Junyaprasert, Varaporn Buraphacheep
Polymer, 2010 , vol. 51, # 11 p. 2286 - 2295
反应条件
sodium carbonate 0.5 h;
参考文献
Gademann; Kimmerlin; Hoyer; Seebach
Journal of Medicinal Chemistry, 2001 , vol. 44, # 15 p. 2460 - 2468
反应条件
sodium carbonate in water T=20°C; 3 h;
参考文献
Zhang, Qi; Chen, Kai; Rao, Weihao; Zhang, Yuejun; Chen, Fa-Jie; Shi, Bing-Feng
Angewandte Chemie - International Edition, 2013 , vol. 52, # 51 p. 13588 - 13592
Angew. Chem., 2013 , vol. 125, # 51 p. 13833 - 13837,5
反应条件
sodium carbonate in ethyl acetate
参考文献
Aitken, R. Alan; Cooper, Harris R.; Mehrotra, Amit P.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 5 p. 475 - 483
反应条件
sodium carbonate in ethyl acetate
参考文献
Aitken, R. Alan; Cooper, Harris R.; Mehrotra, Amit P.
Journal of the Chemical Society - Perkin Transactions 1, 1996 , # 5 p. 475 - 483
反应条件
1.1: sodium carbonate / water / 3 h / 20 °C 2.1: N,N-dimethyl-formamide; thionyl chloride / dichloromethane / 4 h / |Reflux 3.1: N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / -20 °C 4.1: palladium diacetate; CuF2; N,N'-dimethyl-N,N'-propyleneurea / acetone / 24 h / 100 °C / |Inert atmosphere; |Schlenk technique 5.1: sodium nitrite; acetic acid / acetic anhydride / 48.5 h / -15 °C 5.2: 2 h / -15 °C 5.3: 2 h / 0 °C View Scheme
参考文献
Zhang, Qi; Chen, Kai; Rao, Weihao; Zhang, Yuejun; Chen, Fa-Jie; Shi, Bing-Feng
Angewandte Chemie - International Edition, 2013 , vol. 52, # 51 p. 13588 - 13592
Angew. Chem., 2013 , vol. 125, # 51 p. 13833 - 13837,5
参考文献
Matsumura, Eiko; Shin, Takashi; Murao, Sawao; Kawano, Tatsu
Agricultural and Biological Chemistry, 1985 , vol. 49, # 4 p. 973 - 980
反应条件
hydrogenchloride; sodium carbonate in water 1 h; Ambient temperaturepH 9;
参考文献
Journal of the American Chemical Society, , vol. 104, # 18 p. 4934 - 4943