4-甲氧基-2-甲基-1-甲砜苯合成路线 (共 7 条)
反应条件
1: 1-bromo-4-methoxy-2-methylbenzene With n-butyllithium in tetrahydrofuran; hexane T=-78°C; 1 h; 2: dimethyl-disulfide in tetrahydrofuran; hexane T=20°C; 2 h; 3: With water; ammonium chloride in tetrahydrofuran; hexane
参考文献
SYNGENTA PARTICIPATIONS AG,
Patent: WO2009/30467 A2, 2009 ;
Location in patent: Page/Page column 107-108 ;
反应条件
potassium hydroxide in methanol 16 h; Heating;
参考文献
Jacob III; Shulgin
Journal of Medicinal Chemistry, 1983 , vol. 26, # 5 p. 746 - 752
参考文献
Shah; Bhatt; Kanga
Journal of the Chemical Society, 1933 , p. 1375,1379
Journal of the University of Bombay, Science: Physical Sciences, Mathematics, Biological Sciences and Medicine, 1934 , vol. 3/2, p. 155
Full Text Show Details
Suter; McKenzie
Journal of the American Chemical Society, 1934 , vol. 56, p. 2470
参考文献
Torrisi, Stefano; Sortino, Salvatore
Journal of Agricultural and Food Chemistry, 2004 , vol. 52, # 19 p. 5943 - 5949
参考文献
Suter; McKenzie
Journal of the American Chemical Society, 1934 , vol. 56, p. 2470
反应条件
hydrogen bromide; acetic acid T=120 - 130°C;
参考文献
Suter; McKenzie
Journal of the American Chemical Society, 1934 , vol. 56, p. 2470
参考文献
Suter; McKenzie
Journal of the American Chemical Society, 1934 , vol. 56, p. 2470