3-(环己烯-1-基)甲苯合成路线 （共 7 条）
反应条件
acetic acid T=118°C; 1 h;
参考文献
Rono, Lydia J.; Yayla, Hatice G.; Wang, David Y.; Armstrong, Michael F.; Knowles, Robert R.
Journal of the American Chemical Society, 2013 , vol. 135, # 47 p. 17735 - 17738
反应条件
1.1: magnesium; iodine / diethyl ether / 0.5 h / 0 - 20 °C / |Inert atmosphere 1.2: 20 °C / |Inert atmosphere 2.1: acetic acid / 1 h / 118 °C View Scheme
参考文献
Rono, Lydia J.; Yayla, Hatice G.; Wang, David Y.; Armstrong, Michael F.; Knowles, Robert R.
Journal of the American Chemical Society, 2013 , vol. 135, # 47 p. 17735 - 17738
反应条件
1.1: magnesium; iodine / diethyl ether / 0.5 h / 0 - 20 °C / |Inert atmosphere 1.2: 20 °C / |Inert atmosphere 2.1: acetic acid / 1 h / 118 °C View Scheme
参考文献
Rono, Lydia J.; Yayla, Hatice G.; Wang, David Y.; Armstrong, Michael F.; Knowles, Robert R.
Journal of the American Chemical Society, 2013 , vol. 135, # 47 p. 17735 - 17738
反应条件
palladium diacetate; sodium acetate in water T=225°C; P=75006 - 150012 Torr; 0.333333 h; stainless steel reactor; Product distribution;
参考文献
Gron; Tinsley
Tetrahedron Letters, 1999 , vol. 40, # 2 p. 227 - 230
参考文献
Shirakawa, Eiji; Watabe, Ryo; Murakami, Takuya; Hayashi, Tamio
Chemical Communications, 2013 , vol. 49, # 45 p. 5219 - 5221
反应条件
(i) Mg, Et2O, (ii) /BRN= 385735/, (iii) TsOH, benzene; Multistep reaction;
参考文献
Davies,M.T. et al.
Tetrahedron, 1962 , vol. 18, p. 751 - 761
反应条件
palladium on activated charcoal T=300°C; Dehydrierung;
参考文献
Walling; Miller
Journal of the American Chemical Society, 1957 , vol. 79, p. 4181,4185
