potassium tert-butylate in dimethyl sulfoxide
T=20 - 25°C; 48 h;
参考文献
De Meijere, Armin; Von Seebach, Malte; Kozhushkov, Sergei I.; Boese, Roland; Blaeser, Dieter; Cicchi, Stefano; Dimoulas, Tula; Brandi, Alberto
European Journal of Organic Chemistry, 2001 , # 20 p. 3789 - 3795
potassium tert-butylate in dimethyl sulfoxide
T=20 - 25°C; 96 h;
参考文献
De Meijere, Armin; Von Seebach, Malte; Kozhushkov, Sergei I.; Boese, Roland; Blaeser, Dieter; Cicchi, Stefano; Dimoulas, Tula; Brandi, Alberto
European Journal of Organic Chemistry, 2001 , # 20 p. 3789 - 3795
1: 99 percent / Ti(iPrO)4 / diethyl ether / 3 h / 20 - 25 °C
2: 85 percent / pyridine / 168 h / 0 - 5 °C
3: 6 percent / tBuOK / dimethylsulfoxide / 48 h / 20 - 25 °C
View Scheme
参考文献
De Meijere, Armin; Von Seebach, Malte; Kozhushkov, Sergei I.; Boese, Roland; Blaeser, Dieter; Cicchi, Stefano; Dimoulas, Tula; Brandi, Alberto
European Journal of Organic Chemistry, 2001 , # 20 p. 3789 - 3795
