1-(4'-硝基苯基)丙-2-烯-1-酮合成路线 （共 14 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran
T=65°C; Stille coupling; 1 h;
参考文献
Aranha, Rachel M.; Bowser, Amy M.; Madalengoitia, Jose S.
Organic Letters, 2009 , vol. 11, # 3 p. 575 - 578
反应条件
toluene-4-sulfonic acid in acetonitrile
T=0 - 5°C;
参考文献
Miyauchi, Kazuo; Hori, Kimiaki; Hirai, Tsuguji; Takebayashi, Matsuji; Ibata, Toshikazu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 7 p. 2142 - 2146
反应条件
sulfuric acid; nitrogen in tetrahydrofuran; water; toluene; acetonitrile
参考文献
Trustees of The University of Pennsylvania
Patent: US5399790 A1, 1995 ;
反应条件
benzoylchlorobis(triphenylphosphine)palladium(II) in chloroform
T=65°C; 0.33 h;
参考文献
Labadie, Jeff W.; Tueting, David; Stille, J. K.
Journal of Organic Chemistry, 1983 , vol. 48, # 24 p. 4634 - 4642
反应条件
dichloro bis(acetonitrile) palladium(II)
T=30°C; 0.5 h; Product distribution;
参考文献
Bumagin, N. A.; Pomonarev, A. B.; Beletskaya, I. P.
Doklady Chemistry, 1986 , vol. 291, p. 471 - 474
Dokl. Akad. Nauk SSSR Ser. Khim., 1986 , vol. 291, # 4 p. 868 - 872
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; 1 h;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Kashin, A. N.; Beletskaya, I. P.
Doklady Chemistry, 1981 , vol. 261, p. 532 - 535
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 261, # 5 p. 1141 - 1144
反应条件
N-methylanilinium trifluoroacetate in tetrahydrofuran
10 h; Inert atmosphereReflux;
参考文献
Yang, Tang-Po; Li, Qiang; Lin, Jin-Hong; Xiao, Ji-Chang
Chemical Communications, 2014 , vol. 50, # 9 p. 1077 - 1079
反应条件
bis(η3-allyl-μ-chloropalladium(II)) in N,N,N',N',N'',N''-hexamethylphosphoric triamide
T=20°C; 1 h;
参考文献
Bumagin, N. A.; Bumagina, I. G.; Kashin, A. N.; Beletskaya, I. P.
Doklady Chemistry, 1981 , vol. 261, p. 532 - 535
Dokl. Akad. Nauk SSSR Ser. Khim., 1981 , vol. 261, # 5 p. 1141 - 1144
反应条件
1: Et3N / 0 °C
2: 13 percent / TsOH*H2O / acetonitrile / 0 - 5 °C
View Scheme
参考文献
Miyauchi, Kazuo; Hori, Kimiaki; Hirai, Tsuguji; Takebayashi, Matsuji; Ibata, Toshikazu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 7 p. 2142 - 2146
反应条件
in water; acetonitrile
T=0 - 5°C;
参考文献
Miyauchi, Kazuo; Hori, Kimiaki; Hirai, Tsuguji; Takebayashi, Matsuji; Ibata, Toshikazu
Bulletin of the Chemical Society of Japan, 1981 , vol. 54, # 7 p. 2142 - 2146
