N,N-二丁基-2-丙烯酰胺合成路线 (共 7 条)
反应条件
triethylamine in dichloromethane T=0 - 20°C; 20 h; Inert atmosphere;
参考文献
Taaning, Rolf H.; Lindsay, Karl B.; Skrydstrup, Troels
Tetrahedron, 2009 , vol. 65, # 52 p. 10908 - 10916
反应条件
sodium hydroxide; hydroquinone T=85 - 88°C;
参考文献
I.G.Farbenind.
Patent: DE752481 , 1939 ;
DRP/DRBP Org.Chem.
反应条件
tetracarbonylnickel(0) T=80°C; Edukt 4:Acrylsaeure;
参考文献
Rohm and Haas Co.
Patent: US2773063 , 1954 ;
反应条件
in benzene T=5 - 15°C; Acylation; 0.5 h;
参考文献
Kazakov; Kazantsev; Shirshin; Danov; Igolkin; Afon'shin
Russian Journal of Applied Chemistry, 2000 , vol. 73, # 5 p. 912 - 913
参考文献
Erickson
Journal of the American Chemical Society, 1952 , vol. 74, p. 6281
参考文献
Ratchford; Lengel; Fisher
Journal of the American Chemical Society, 1949 , vol. 71, p. 648,650
反应条件
NiCl2((PPh3)P)2; BFBED; iron; potassium iodide in N,N-dimethyl acetamide; toluene
T=90°C; 120 h; Schlenk techniqueSealed tubeInert atmosphere;
参考文献
Meng, Jing-Jing; Gao, Min; Dong, Min; Wei, Yu-Ping; Zhang, Wen-Qin
Tetrahedron Letters, 2014 , vol. 55, # 13 p. 2107 - 2109