反应条件
1: para-iodoanisole; acetylenecarboxylic acid With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine in N,N-dimethyl-formamide
T=20°C; Sonogashira coupling; 6 h; Inert atmosphereSealed tube;
2: 3-phenyl-2-propynoic acid With triethylamine; silver carbonate in N,N-dimethyl-formamide
T=130°C; 20 h; Inert atmosphereSealed tube;
参考文献
Park, Jihye; Park, Eonjeong; Kim, Aejin; Park, Seul-A; Lee, Youngil; Chi, Ki-Whan; Jung, Young Hoon; Kim, In Su
Journal of Organic Chemistry, 2011 , vol. 76, # 7 p. 2214 - 2219
