2-(3-氯苯基)苯并[d]噻唑合成路线 （共 22 条）
反应条件
Iron (III) nitrate nonahydrate; oxygen; [(t-Bu)3PH]BF4 in water; dimethyl sulfoxide
T=120°C; 24 h; Sealed tubeGreen chemistry;
参考文献
Khemnar, Ashok B.; Bhanage, Bhalchandra M.
RSC Advances, 2014 , vol. 4, # 18 p. 8939 - 8942
反应条件
tetrabutylammomium bromide; silver(I) acetate; palladium diacetate; potassium carbonate in N,N-dimethyl-formamide
T=120°C; 18 h; Molecular sieveInert atmosphere;
参考文献
Saha, Debasree; Adak, Laksmikanta; Ranu, Brindaban C.
Tetrahedron Letters, 2010 , vol. 51, # 42 p. 5624 - 5627
反应条件
copper(l) iodide; 1,10-phenanthroline; Na2S*9H2O in acetic acid
T=100°C; 12 h; Sealed tube;
参考文献
Liu, Jidan; Gui, Qingwen; Yang, Zhiyong; Tan, Ze; Guo, Ruqing; Shi, Ji-Cheng
Synthesis (Germany), 2013 , vol. 45, # 7 art. no. SS-2012-F0968-OP, p. 943 - 951
反应条件
dipotassium peroxodisulfate; potassium tert-butylate in water; dimethyl sulfoxide
T=100°C; 8 h;
参考文献
Yang, Zhiyong; Wang, Anwei; Chen, Xiang; Gui, Qingwen; Liu, Jidan; Tan, Ze; Wang, Hua; Shi, Ji-Cheng
Synlett, 2013 , vol. 24, # 12 art. no. ST-2013-W0351-L, p. 1549 - 1554
反应条件
sodium dithionite in dimethyl sulfoxide
T=80°C; 8 h; Molecular sieve;
参考文献
Wang, Zhanglin; Tang, Riyuan; Xiao, Qin
Chinese Journal of Chemistry, 2011 , vol. 29, # 2 p. 314 - 320
反应条件
triethyl amine hydrochloride
T=180°C; 3.5 h;
参考文献
Ohno; Mizukoshi; Izumi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1988 , vol. 36, # 2 p. 551 - 562
反应条件
triethyl amine hydrochloride
T=150°C; Heating;
参考文献
Ohno; Izumi; Mizukoshi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 5 p. 1780 - 1783
反应条件
1: isopentyl nitrite / tetrahydrofuran / 0.5 h / |Reflux
2: FeCl3·6H2O; dipotassium peroxodisulfate / dimethyl sulfoxide; water / 12 h / 100 °C
View Scheme
参考文献
Wang, Jian; Zhang, Xiao-Zhuan; Chen, Shan-Yong; Yu, Xiao-Qi
Tetrahedron, 2014 , vol. 70, # 2 p. 245 - 250
反应条件
1: Ambient temperature
2: triethylamine hydrochloride / 150 °C / Heating
View Scheme
参考文献
Ohno; Izumi; Mizukoshi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 5 p. 1780 - 1783
反应条件
1: Ambient temperature
2: triethylamine hydrochloride / 150 °C / Heating
View Scheme
参考文献
Ohno; Izumi; Mizukoshi; Kato; Hori
Chemical and Pharmaceutical Bulletin, 1983 , vol. 31, # 5 p. 1780 - 1783
