2-吡啶-3-基-1,3-苯并恶唑合成路线 （共 27 条）
反应条件
1: methanol / 12 h / 45 °C 2: 74 percent / DDQ / CH2Cl2 / 0.5 h / 20 °C View Scheme
参考文献
Chang, Junbiao; Zhao, Kang; Pan, Shifeng
Tetrahedron Letters, 2002 , vol. 43, # 6 p. 951 - 954
反应条件
1: palladium diacetate; di-(1-adamantyl)-n-butylphosphine; ammonia / 1,4-dioxane / 16 h / 100 °C / 1500.15 Torr / |Autoclave 2: copper(l) iodide; N-methyl-2-(methylamino)ethylamine; potassium carbonate / 1,4-dioxane / 20 h / 110 °C View Scheme
参考文献
Wu, Xiao-Feng; Neumann, Helfried; Neumann, Stephan; Beller, Matthias
Tetrahedron Letters, 2013 , vol. 54, # 24 p. 3040 - 3042
参考文献
Rips,R. et al.
Chimica Therapeutica, 1971 , vol. 6, p. 126 - 130
反应条件
in water; acetonitrile photosubstitution; photoreduction; 1.5 h; UV-irradiation; Kinetics; Further Variations:Reagents;
参考文献
Park, Yong-Tae; Jung, Chang-Hee; Kim, Kwang-Wook; Kim, Ho Sik
Journal of Organic Chemistry, 1999 , vol. 64, # 23 p. 8546 - 8556
反应条件
sulfuric acid; nitric acid
2 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Haugwitz; Angel; Jacobs; Maurer; Narayanan; Cruthers; Szanto
Journal of Medicinal Chemistry, 1982 , vol. 25, # 8 p. 969 - 974
反应条件
1: HNO3, H2SO4 / 2 h / Ambient temperature
2: H2 / PtO2 / ethanol / 2585.7 Torr
View Scheme
参考文献
Haugwitz; Angel; Jacobs; Maurer; Narayanan; Cruthers; Szanto
Journal of Medicinal Chemistry, 1982 , vol. 25, # 8 p. 969 - 974
反应条件
1: HNO3, H2SO4 / 2 h / Ambient temperature
2: H2 / PtO2 / ethanol / 2585.7 Torr
3: Et3N / tetrahydrofuran / 24 h / Heating
View Scheme
参考文献
Haugwitz; Angel; Jacobs; Maurer; Narayanan; Cruthers; Szanto
Journal of Medicinal Chemistry, 1982 , vol. 25, # 8 p. 969 - 974
