3-(4-羟基-3-甲氧基苯基)-1-丙醇合成路线 (共 22 条)
反应条件
hydrogen T=150°C; P=15514.9 Torr; 2 h; Sealed tube;
参考文献
Chemical Science, , vol. 4, # 2 p. 806 - 813
反应条件
sodium tetrahydroborate in ethyl acetate 1 h; Ambient temperature;
参考文献
Journal of Agricultural and Food Chemistry, , vol. 44, # 10 p. 2942 - 2943
反应条件
sodium sulfide; sodium hydroxide T=135°C;
参考文献
Chemische Berichte, , vol. 99, p. 2638 - 2651
反应条件
T=165°C; P=154457 Torr; Hydrogenation;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 63,64, 66
反应条件
sodium hydroxide; dimethylsulfide; borane; dihydrogen peroxide other reagents: borane/THF, 9-borabicyclo<3.3.1>nonane; Multistep reaction;
参考文献
Bioorganic and Medicinal Chemistry Letters, , vol. 7, # 24 p. 3081 - 3084
参考文献
Sci. Rep. Tohoku Univ., Ser. 1: Phys., Chem., Astron., vol. 17, p. 694
Chem.Abstr., , p. II, 1325
参考文献
Monatshefte fuer Chemie, , vol. 94, p. 530 - 536
Bulletin of the Agricultural Chemical Society of Japan, , vol. 21, p. 250
反应条件
boron trifluoride diethyl etherate; silica gel T=20°C; 9 h;
参考文献
Das, Biswanath; Venkataiah; Madhusudhan
Synthetic Communications, 2002 , vol. 32, # 2 p. 249 - 252
反应条件
boron trifluoride diethyl etherate in tetrahydrofuran Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Hutchinson, Sally A.; Luetjens, Henning; Scammells, Peter J.
Bioorganic and Medicinal Chemistry Letters, 1997 , vol. 7, # 24 p. 3081 - 3084
反应条件
dimethyl sulfoxide; triethylamine in dichloromethane
T=20°C; 0.5 h;
参考文献
Kasahara, Hiroyuki; Jiao, Ying; Bedgar, Diana L.; Kim, Sung-Jin; Patten, Ann M.; Xia, Zhi-Qiang; Davin, Laurence B.; Lewis, Norman G.
Phytochemistry, 2006 , vol. 67, # 16 p. 1765 - 1780