3,3,5-三苯基-1,2,4-三氧杂环戊烷合成路线 （共 13 条）
反应条件
biphenyl; 9,10-anthracenedicarbonitrile; oxygen in acetonitrile T=10°C; 0.666667 h; Irradiation;
参考文献
Schaap, A. Paul; Siddiqui, Shahabuddin; Prasad, Girija; Palomino, Eduardo; Sandison, Mark
Tetrahedron, 1985 , vol. 41, # 11 p. 2229 - 2236
反应条件
oxygen; P-Rose Bengal in acetonitrile T=2°C; 0.666667 h; Irradiation;
参考文献
Murray, Robert W.; Morgan, Michael M.
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 684 - 687
反应条件
1: 80 percent / activated MnO2, anhydrous MgSO4 / CH2Cl2 / 1) 0 deg C, 2 h, 2) r.t., 1 h 2: 30.26 percent / oxygen / P-Rose Bengal / acetonitrile / 0.67 h / 2 °C / Irradiation View Scheme
参考文献
Murray, Robert W.; Morgan, Michael M.
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 684 - 687
反应条件
ozone in dichloromethane Ambient temperature;
参考文献
Murray, Robert W.; Morgan, Michael M.
Journal of Organic Chemistry, 1991 , vol. 56, # 2 p. 684 - 687
反应条件
in acetonitrile T=70°C; relative rate constant, various reactants ratio, relative intensity of chemiluminescence; Mechanism;
参考文献
Nazarov; Yamilova; Khursan; Komissarov
Russian Chemical Bulletin, 1998 , vol. 47, # 11 p. 2129 - 2133
反应条件
1: boron trifluoride-diethyl ether / CH2Cl2 / 0.33 h / 0 °C 2: 15 percent Chromat. / lithium aluminum hydride / diethyl ether / 2 h / Heating View Scheme
参考文献
Yoshida; Miura; Nojima; Kusabayashi
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6279 - 6285
反应条件
antimony(V) pentachloride in dichloromethane 0.5 h; Ambient temperaturefurther reagent; Yield given. Yields of byproduct given;
参考文献
Miura,M.; Nojima,M.
Journal of the American Chemical Society, 1980 , vol. 102, p. 288
反应条件
1: boron trifluoride-diethyl ether / CH2Cl2 / 0.33 h / 0 °C 2: 60 percent Chromat. / lithium aluminum hydride / diethyl ether / 2 h View Scheme
参考文献
Yoshida; Miura; Nojima; Kusabayashi
Journal of the American Chemical Society, 1983 , vol. 105, # 20 p. 6279 - 6285
反应条件
chlorosulfonic acid 80 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2909 - 2913
反应条件
chlorosulfonic acid in methanol 80 h;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , p. 2909 - 2913
