(S,S)-(-)-氢化苯偶姻合成路线 (共 230 条)
反应条件
1-phenyl-1H-pyrrole; FeCl3·6H2O; dihydrogen peroxide in water; acetone T=25 - 62°C; In air; chemoselective reaction;
参考文献
Green Chemistry, , vol. 13, # 5 p. 1230 - 1237
反应条件
Bacillus megaterium ECU1001 cell-free extract in potassium phosphate buffer; dimethyl sulfoxide T=30°C; pH=7; 0.166667 h; Resolution of racemateEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Advanced Synthesis and Catalysis, , vol. 353, # 9 p. 1510 - 1518
反应条件
D-glucose in N,N-dimethyl-formamide T=20°C; electrolysis, var. of reagent; Product distribution;
参考文献
Journal of the Chemical Society, Chemical Communications, , # 10 p. 492 - 494
反应条件
lithium sulphate; sulfuric acid in methanol; water Ambient temperatureelectrolysis in membrane flow cell with a Pb cathode;
参考文献
Acta Chemica Scandinavica, , vol. 52, # 1 p. 32 - 36
反应条件
1: With [Rh(COD)(dppp)]BF4; benzo[1,3,2]dioxaborole in tetrahydrofuran T=25°C; 2 h; 2: With sodium hydroxide; dihydrogen peroxide in ethanol
参考文献
Tetrahedron Asymmetry, , vol. 16, # 7 p. 1289 - 1294
反应条件
PTAB; antimony(III)tribromide in dimethyl sulfoxide T=20°C; 40 h; Product distribution; Further Variations:ReagentsSolventsreaction times, reagent ratios;
参考文献
Sayama, Shinsei
Tetrahedron Letters, 2006 , vol. 47, # 24 p. 4001 - 4005
反应条件
manganese; titanium tetrachloride in tetrahydrofuran T=-10°C; 0.4 h; Inert atmosphere;
参考文献
Synthesis, , # 2 p. 277 - 282
反应条件
manganese; titanium tetrachloride in tetrahydrofuran T=-10°C; 0.366667 h; Inert atmosphere;
参考文献
Synthesis, , # 2 p. 277 - 282
反应条件
manganese; titanium tetrachloride in tetrahydrofuran T=-10°C; 0.5 h; Inert atmosphere;
参考文献
Synthesis, , # 2 p. 277 - 282
反应条件
1: With manganese; triethylsilyl chloride; C46H38ClCrN2O2 in tetrahydrofuran T=40°C; Nozaki-Hiyama propargylation; 40 h; Inert atmosphere; 2: With tetrabutyl ammonium fluoride in tetrahydrofuran T=22°C; 1 h; Inert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Angewandte Chemie - International Edition, , vol. 49, # 44 p. 8169 - 8172