(S,S)-(-)-氢化苯偶姻合成路线 (共 230 条)
反应条件
samarium diiodide; magnesium; ethylene dibromide in tetrahydrofuran T=20°C; Reformatsky reaction;
参考文献
Tetrahedron Letters, , vol. 46, # 11 p. 1909 - 1911
反应条件
samarium diiodide; phosphoric acid in tetrahydrofuran T=20°C; 0.000833333 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 53, # 8 p. 1017 - 1020
反应条件
tetrabutyl ammonium fluoride in N,N,N',N',N'',N''-hexamethylphosphoric triamide byproducts: Me3GeH; (Ar); stirring at room temp. for 4.5 h in hexamethylphosporamide (HMPA); addn. of HCl/MeOH; mixed with ether; washed with water and aq. NaCl-soln.; dried over MgSO4; concd.; chromd. on silica gel column (hexane/ethyl acetate); elem. anal.;
参考文献
Synthetic Communications, , vol. 20, # 20 p. 3245 - 3252
反应条件
chloro-trimethyl-silane; titanium (IV) isopropoxide; magnesium; triethylamine in tetrahydrofuran T=40°C; McMurry coupling; 48 h; optical yield given as percent de;
参考文献
Okamoto, Sentaro; He, Jing-Qian; Ohno, Chihaya; Oh-iwa, Yuhji; Kawaguchi, Yuhki
Tetrahedron Letters, 2010 , vol. 51, # 2 p. 387 - 390
反应条件
graphite; potassium bromide in water T=25°C; Electrolysis;
参考文献
Electrochimica Acta, , vol. 132, p. 118 - 126
反应条件
oxone; BLM (iron-bleomycin complex); iron(III) cation in water; acetonitrile 1 h; Ambient temperature; Yield given. Further byproducts given;
参考文献
Tetrahedron Letters, , vol. 28, # 26 p. 2955 - 2958
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide in tetrahydrofuran 30 h; Ambient temperature;
参考文献
Chemistry Letters, , # 6 p. 959 - 962
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; samarium diiodide; 2,3-butadione in tetrahydrofuran 30 h; Ambient temperature;
参考文献
Chemistry Letters, , # 6 p. 959 - 962
反应条件
dodecacarbonyltriiron in pyridine T=80°C; 20 h;
参考文献
Chemistry Letters, , p. 1141 - 1144
反应条件
hydroquinone in N,N-dimethyl-formamide cathodic reduction, vitreous carbon cathode, (E = -2.20 V);
参考文献
Journal of Chemical Research, Miniprint, , # 12 p. 3355 - 3368