sulfuryl dichloride; acetic anhydride in dichloromethane T=0 - 5°C;
参考文献
Block, Eric; Gillies, Jennifer Z.; Gillies, Charles W.; Bazzi, Ali A.; Putman, David; Revelle, Larry K.; Wang, Dongyi; Zhang, Xing
Journal of the American Chemical Society, 1996 , vol. 118, # 32 p. 7492 - 7501
in not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.;
参考文献
Narula, Suraj P.; Sharma, R. K.; Lata, Sneh; Walia, Rita
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical, 1983 , vol. 22, # 3 p. 246 - 247
in not given dropwise addn. of thionyl chloride to tetraalkyltin(IV) compd. under dry N2 atmosphere under ice cooling, warming to room temp., refluxing for 30 min; distn. (removal of excess of SOCl2), cooling resulting liquids, sepn., elem. anal.;
参考文献
Narula, Suraj P.; Sharma, R. K.; Lata, Sneh; Walia, Rita
Indian Journal of Chemistry, Section A: Inorganic, Physical, Theoretical and Analytical, 1983 , vol. 22, # 3 p. 246 - 247
