苯并[g][1]苯并二硫杂环戊烷合成路线 （共 42 条）
反应条件
T=600°C; 0.0158333 h; gas phase copyrolysis; Product distribution;
参考文献
Voronkov, M. G.; Deryagina, E. N.; Sukhomazova, E. N.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1516 - 1522
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 8 p. 1736 - 1743
反应条件
T=580°C; other naphthol derivatives, var. temp.; also 1-halonaphthalenes with H2S; Product distributionMechanism;
参考文献
Russavskaya, N. V.; Sukhomazova, E. N.; Korchevin, N. A.; Deryagina, E. N.; Voronkov, M. G.
Journal of Organic Chemistry USSR (English Translation), 1991 , vol. 27, # 8 p. 1531 - 1534
Zhurnal Organicheskoi Khimii, 1991 , vol. 27, # 8 p. 1743 - 1747
反应条件
trifluorormethanesulfonic acid in dichloromethane
T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Rafiq, Settu Muhamad; Sivasakthikumaran, Ramakrishnan; Mohanakrishnan, Arasambattu K.
Organic Letters, 2014 , vol. 16, # 10 p. 2720 - 2723
反应条件
aluminium trichloride in 1,2-dichloro-ethane
4.5 h; Ambient temperature;
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 71 percent / AlCl3 / 1,2-dichloro-ethane / 4.5 h / Ambient temperature
2: 70 percent / zinc dust, conc. ammonium hydroxide / 24 h / Heating
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 71 percent / AlCl3 / 1,2-dichloro-ethane / 4.5 h / Ambient temperature
2: 70 percent / zinc dust, conc. ammonium hydroxide / 24 h / Heating
3: 76 percent / LiAlH4 / diethyl ether / 3.5 h / Ambient temperature
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
1: 71 percent / AlCl3 / 1,2-dichloro-ethane / 4.5 h / Ambient temperature
2: 70 percent / zinc dust, conc. ammonium hydroxide / 24 h / Heating
3: 76 percent / LiAlH4 / diethyl ether / 3.5 h / Ambient temperature
4: CrO3 / pyridine / 2.5 h / Ambient temperature
View Scheme
参考文献
Tedjamulia, Marvin L.; Tominaga, Yoshinori; Castle, Raymond N.; Lee, Milton L.
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1143 - 1148
反应条件
aluminium trichloride; nickel
1.) benzene, 20 deg C, 4 h; 2.) aq. EtOH, 18 h, reflux; Multistep reaction. Title compound not separated from byproducts;
参考文献
Clark, Peter David; McKinnon, David M.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 1297 - 1302
反应条件
aluminium trichloride; nickel
1.) 20 deg C, 4 h; 2.) aq. EtOH, 18 h, reflux; Multistep reaction. Title compound not separated from byproducts;
参考文献
Clark, Peter David; McKinnon, David M.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 1297 - 1302
反应条件
aluminium trichloride in ethylbenzene
T=136°C; 2 h;
参考文献
Clark, Peter David; McKinnon, David M.
Canadian Journal of Chemistry, 1981 , vol. 59, p. 1297 - 1302
