1: 11.5 g / tetrahydrofuran / 1 h / -78 °C
2: 4.5 percent / Zn-Ag / methanol; diethyl ether / 18 h
3: 94 percent / diisobutylaluminum hydride / hexane; toluene / 4 h / -78 °C
View Scheme
参考文献
Paquette, Leo A.; Gardlik, John M.; McCullough, Kevin J.; Samodral, Rodney; DeLucca, George; Ouellette, Robert J.
Journal of the American Chemical Society, 1983 , vol. 105, # 26 p. 7649 - 7655
1: 79 percent / diethyl ether / 1.) -38 deg C to -25 deg C, 1 h, 2.) room temperature, 1 h
2: 70 percent / selenium dioxide / 2-methyl-propan-2-ol / 48 h / Heating
View Scheme
参考文献
Smith, Amos B.; Levenberg, Patricia A.; Jerris, Paula J.; Scarborough, Robert M.; Wovkulich, Peter M.
Journal of the American Chemical Society, 1981 , vol. 103, # 6 p. 1501 - 1513
in diethyl ether
1.) -38 deg C to -25 deg C, 1 h, 2.) room temperature, 1 h;
参考文献
Smith, Amos B.; Levenberg, Patricia A.; Jerris, Paula J.; Scarborough, Robert M.; Wovkulich, Peter M.
Journal of the American Chemical Society, 1981 , vol. 103, # 6 p. 1501 - 1513
Kitamura, Tsugio; Tanaka, Toshimasa; Taniguchi, Hiroshi; Stang, Peter J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1991 , # 11 p. 2892 - 2893
