2-氨基-5-硝基苯硫醇合成路线 （共 18 条）
反应条件
1: methanol. sodium methylate
2: aqueous KOH-solution
View Scheme
参考文献
Colonna; Andrisano
Bollettino Scientifico della Facolta di Chimica Industriale di Bologna, 1943 , vol. 4, p. 70
参考文献
Mylius
Dissertation <Berlin 1883>, S. 48
反应条件
hydrogenchloride; tin
参考文献
Mylius
Dissertation <Berlin 1883>,S.51
反应条件
1: 67.1 percent / pyridine / 20 h / Heating
2: 68.8 percent / tin(II) chloride dihydrate; HCl / methanol / 0.25 h / Heating
View Scheme
参考文献
Racane, Livio; Stojkovic, Ranko; Tralic-Kulenovic, Vesna; Karminski-Zamola, Grace
Molecules, 2006 , vol. 11, # 5 p. 325 - 333
参考文献
Pan, Jinhe; Mason, Neale S.; Debnath, Manik L.; Mathis, Chester A.; Klunk, William E.; Lin, Kuo-Shyan
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1720 - 1726
反应条件
1: N,N-dimethyl-formamide / 18 h / 140 °C
2: tin(ll) chloride; ethanol / 3 h / |Reflux
View Scheme
参考文献
Pan, Jinhe; Mason, Neale S.; Debnath, Manik L.; Mathis, Chester A.; Klunk, William E.; Lin, Kuo-Shyan
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1720 - 1726
反应条件
in pyridine
20 h; Heating;
参考文献
Racane, Livio; Stojkovic, Ranko; Tralic-Kulenovic, Vesna; Karminski-Zamola, Grace
Molecules, 2006 , vol. 11, # 5 p. 325 - 333
反应条件
1: N,N-dimethyl-formamide / 18 h / 140 °C
2: tin(ll) chloride; ethanol / 3 h / |Reflux
View Scheme
参考文献
Pan, Jinhe; Mason, Neale S.; Debnath, Manik L.; Mathis, Chester A.; Klunk, William E.; Lin, Kuo-Shyan
Bioorganic and Medicinal Chemistry Letters, 2013 , vol. 23, # 6 p. 1720 - 1726
