2,2-二甲基丙基4-甲基苯磺酸酯合成路线 (共 30 条)
反应条件
pyridine 1.) 0 deg C, 30 min 2.) 20 deg C, 3 h;
参考文献
Courtin, Alfred; Tobel, Hans-Rudolf von; Auerbach, Guenther
Helvetica Chimica Acta, 1980 , vol. 63, # 6 p. 1412 - 1419
反应条件
in toluene T=110°C; 24 h;
参考文献
King,J.F.; Loosmore,S.M.; Aslam,M.
Journal of the American Chemical Society, 1982 , vol. 104, p. 7108
反应条件
1: CH2Cl2 / 0.17 h 2: 99 percent / CH2Cl2 3: 2 percent / toluene / 24 h / 110 °C View Scheme
参考文献
King,J.F.; Loosmore,S.M.; Aslam,M.
Journal of the American Chemical Society, 1982 , vol. 104, p. 7108
反应条件
1: 99 percent / CH2Cl2 2: 2 percent / toluene / 24 h / 110 °C View Scheme
参考文献
King,J.F.; Loosmore,S.M.; Aslam,M.
Journal of the American Chemical Society, 1982 , vol. 104, p. 7108
反应条件
in chloroform-d1 T=20°C; 48 h; Further byproducts given;
参考文献
Hao, Wei; Fujii, Takayoshi; Dong, Tiaoling; Wakai, Youko; Yoshimura, Toshiaki
Heteroatom Chemistry, 2004 , vol. 15, # 3 p. 193 - 198
反应条件
sodium methylate in ethanol; water T=75°C; 45, 55 deg C; Rate constant;
参考文献
Roberts, Donald D.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2521 - 2526
反应条件
in tetrahydrofuran other arenesulfonate esters; var. solvents, temp.; Product distributionMechanism;
参考文献
Journal of Organic Chemistry, , vol. 47, # 12 p. 2476 - 2479
反应条件
sodium methylate in ethanol; water T=75°C; 45, 55 deg C; Rate constant;
参考文献
Roberts, Donald D.
Journal of Organic Chemistry, 1984 , vol. 49, # 14 p. 2521 - 2526
反应条件
in 2,2,2-trifluoroethanol; water T=45°C; solvolysis; Kinetics; Further Variations:SolventsTemperatures;
参考文献
Roberts
Journal of Organic Chemistry, 1999 , vol. 64, # 4 p. 1341 - 1343
反应条件
1,1'-bis(diphenylphosphanyl)ferrocenenickel(II) chloride in tetrahydrofuran 28 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 68, # 8 p. 3017 - 3025