2-丙基-2,6,7,8-四氢色烯-5-酮合成路线 (共 2 条)
反应条件
1: 3-propylacrolein With piperidine; acetic anhydride in toluene T=85°C; 1 h; 2: 1,3-cylohexanedione in toluene T=150°C; 3 h; Further stages.;
参考文献
Shen, Hong C.; Wang, Jiashi; Cole, Kevin P.; McLaughlin, Michael J.; Morgan, Christopher D.; Douglas, Christopher J.; Hsung, Richard P.; Coverdale, Heather A.; Gerasyuto, Aleksey I.; Hahn, Juliet M.; Liu, Jia; Sklenicka, Heather M.; Wei, Lin-Li; Zehnder, Luke R.; Zificsak, Craig A.
Journal of Organic Chemistry, 2003 , vol. 68, # 5 p. 1729 - 1735
反应条件
4 A molecular sieve in dichloromethane
参考文献
Kurdyumov, Aleksey V.; Lin, Nan; Hsung, Richard P.; Gullickson, Glen C.; Cole, Kevin P.; Sydorenko, Nadiya; Swidorski, Jacob J.
Organic Letters, 2006 , vol. 8, # 2 p. 191 - 193