4-叔-丁基吡啶 1-氧化合成路线 （共 12 条）
反应条件
dihydrogen peroxide; acetic acid in water T=90°C;
参考文献
Hendricks, Robert Than; Hermann, Johannes; Kondru, Rama; Lou, Yan; Lynch, Stephen M.; Owens, Timothy D.; Soth, Michael
Patent: US2011/230462 A1, 2011 ;
Location in patent: Page/Page column 97 ;
US 20110230462 A1
反应条件
titanium tetrachloride; tin(ll) chloride in benzene 0.5 h; Ambient temperature;
参考文献
Kaczmarek, Lukasz; Malinowski, Marek; Balicki, Roman
Bulletin des Societes Chimiques Belges, 1988 , vol. 97, # 10 p. 787 - 790
反应条件
in acetonitrile T=81°C; 4 h;
参考文献
Ponaras, Anthony A.; Zaim, Oemer
Journal of Heterocyclic Chemistry, 2007 , vol. 44, # 2 p. 487 - 489
反应条件
1: (CH3)2NCOCl / CH2Cl2 2: aq. HCl / Heating View Scheme
参考文献
Ko, Po-Hung; Chen, Tai-Yuen; Zhu, Jin; Cheng, Kin-Fai; Peng, Shie-Ming; Che, Chi-Ming
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , # 13 p. 2215 - 2220
反应条件
trichlorophosphate
RefluxInert atmosphere;
参考文献
Fu, Ross; Bercaw, John E.; Labinger, Jay A.
Organometallics, 2011 , vol. 30, # 24 p. 6751 - 6765
反应条件
triethylamine in acetonitrile
T=100°C; 25 h;
参考文献
Custelcean, Radu; Bonnesen, Peter V.; Duncan, Nathan C.; Zhang, Xiaohua; Watson, Lori A.; Van Berkel, Gary; Parson, Whitney B.; Hay, Benjamin P.
Journal of the American Chemical Society, 2012 , vol. 134, # 20 p. 8525 - 8534
反应条件
in chloroform; water; ethyl alcohol water
参考文献
Shiseido Company, Ltd.
Patent: US5219847 A1, 1993 ;
反应条件
1: 95 percent / 3 h / 90 - 100 °C
2: 45 percent / H2O; ethanol / 3 h / -18 - -12 °C
View Scheme
参考文献
Greci, Lucedio; Alberti, Angelo; Carelli, Italo; Trazza, Antonio; Casini, Antonio
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , p. 2013 - 2018
反应条件
dimethyl sulfate
1.) 95 deg C, 3 h, 2.) H2O, r.t., 6 h; Multistep reaction;
参考文献
Ko, Po-Hung; Chen, Tai-Yuen; Zhu, Jin; Cheng, Kin-Fai; Peng, Shie-Ming; Che, Chi-Ming
Journal of the Chemical Society, Dalton Transactions: Inorganic Chemistry (1972-1999), 1995 , # 13 p. 2215 - 2220
反应条件
1: With phosphorus oxytribromide in 1,2-dichloro-ethane
T=20 - 70°C;
2: With water; sodium hydroxide in 1,2-dichloro-ethane
pH=10; Cooling;
参考文献
Hendricks, Robert Than; Hermann, Johannes; Kondru, Rama; Lou, Yan; Lynch, Stephen M.; Owens, Timothy D.; Soth, Michael
Patent: US2011/230462 A1, 2011 ;
Location in patent: Page/Page column 97 ;
US 20110230462 A1
