3-(哌啶-1-基)丙酸甲酯合成路线 (共 18 条)
反应条件
hydrogen fluoride T=7 - 8°C; 8.93333 h; electrochemical fluorination; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 57, p. 101 - 111
反应条件
hydrogen fluoride T=7 - 8°C; 8.93333 h; electrochemical fluorination; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 57, p. 101 - 111
反应条件
hydrogen fluoride T=7 - 8°C; 8.93333 h; electrochemical fluorination; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 57, p. 101 - 111
反应条件
hydrogen fluoride T=7 - 8°C; 8.93333 h; electrochemical fluorination; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Journal of Fluorine Chemistry, , vol. 57, p. 101 - 111
反应条件
lithium aluminium tetrahydride in diethyl ether T=20°C; 2 h;
参考文献
Le Sann, Christine; Huddleston, Jonathan; Mann, John
Tetrahedron, 2007 , vol. 63, # 52 p. 12903 - 12911
反应条件
hydrogen fluoride T=7 - 8°C; 8.93333 h; electrochemical fluorination; Further byproducts given;
参考文献
Abe, Takashi; Hayashi, Eiji; Fukaya, Haruhiko; Hayakawa, Yoshio; Baba, Hajime; et al.
Journal of Fluorine Chemistry, 1992 , vol. 57, p. 101 - 111
反应条件
copper diacetate in water
T=20°C; aza-Michael addition; 12 h;
参考文献
Saidi, Mohammad R.; Pourshojaei, Yaghoub; Aryanasab, Fezzeh
Synthetic Communications, 2009 , vol. 39, # 6 p. 1109 - 1119
参考文献
ITALFARMACO S.p.A.
Patent: EP748310 B1, 1999 ;
反应条件
9,10-anthracenedione in acetonitrile
T=5°C; 2 h; Irradiation; Yields of byproduct given;
参考文献
Das, Suresh; Kumar, J. S. Dileep; Shivaramayya, K.; George, M. V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1995 , # 14 p. 1797 - 1800
反应条件
toluene-4-sulfonic acid
6 h; Heating;
参考文献
Komarova, L. I.; Lomanovskaya, T. D.; Komarov, N. V.
Journal of Organic Chemistry USSR (English Translation), 1982 , vol. 18, p. 1624 - 1627
Zhurnal Organicheskoi Khimii, 1982 , vol. 18, # 9 p. 1857 - 1860