2,5-二甲基己烷-2,5-二胺合成路线 （共 10 条）
反应条件
in water T=300°C; 15 h; Title compound not separated from byproducts;
参考文献
Smith, John R. Lindsay; Smart, Alison U.; Twigg, Martyn V.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1992 , # 6 p. 939 - 947
反应条件
acetic acid; thiourea in ethanol
Heating;
参考文献
Hill, Nicole L.; Braslau, Rebecca
Macromolecules, 2005 , vol. 38, # 22 p. 9066 - 9074
反应条件
sulfuric acid; sodium cyanide; acetic acid
1.) 1h,0-5 deg C; 15h,20-25 deg C; 1h,60-70 deg C; Yield given;
参考文献
Quast, Helmut; Heuschmann, Manfred; Abdel-Rahman, Mohamed O.
Liebigs Annalen der Chemie, 1981 , # 5 p. 943 - 966
反应条件
1: 0.08 h / 40 °C
2: Hydrogen / PtO2
View Scheme
参考文献
Banert, Klaus
Tetrahedron Letters, 1985 , vol. 26, # 43 p. 5261 - 5264
反应条件
1: 28 percent / 0.08 h / 40 °C
2: Hydrogen / PtO2
View Scheme
参考文献
Banert, Klaus
Tetrahedron Letters, 1985 , vol. 26, # 43 p. 5261 - 5264
反应条件
perchloric acid; sodium perchlorate; dihydrogen peroxide; iron(II) sulfate
T=40°C; activation energy 105 KJ mol-1; determination of velocity constants in dependence on temperature, concentration of hydrogen peroxide, and substrate concentration; Rate constantKineticsThermodynamic data;
参考文献
Ahmad, Iftikhar; Rauf, A. M. A.; Saeed, Kamal M.
Journal fuer Praktische Chemie (Leipzig), 1984 , vol. 326, # 1 p. 23 - 28
反应条件
sulfuric acid; water
参考文献
Rohm and Haas Co.
Patent: US2633023 , 1950 ;
参考文献
Coffman et al.
Journal of the American Chemical Society, 1958 , vol. 80, p. 2864,2870
反应条件
3: reduction
View Scheme
参考文献
Weinstock; Rost; Cheng
Journal of Pharmaceutical Sciences, 1981 , vol. 70, # 8 p. 956 - 959
参考文献
Bayer AG
Patent: DE2515146 , 1976 ;
Chem.Abstr., 1977 , vol. 86, # 71947
