3-甲基-1-辛炔-3-醇合成路线 （共 11 条）
反应条件
hydrogen; Lindlar's catalyst in hexane
参考文献
Karavanov, A. N.; Gryaznov, V. M.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 8.1 p. 1593 - 1596
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 8 p. 1740 - 1745
反应条件
diethyl ether; sodium amide
nachfolgenden Einleiten von Acetylen;
参考文献
Leers
Bulletin de la Societe Chimique de France, 1926 , vol. <4>39, p. 423
反应条件
in tetrahydrofuran; toluene; xylene
3 h; Ambient temperature;
参考文献
Joung, Meyoung Ju; Ahn, Jin Hee; Yoon, Nung Min
Journal of Organic Chemistry, 1996 , vol. 61, # 13 p. 4472 - 4475
参考文献
du Pont de Nemours and Co.
Patent: US2106180 , 1936 ;
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Campbell; Campbell; Eby
Journal of the American Chemical Society, 1938 , vol. 60, p. 2882
反应条件
potassium hydroxide
T=6°C; P=2574.3 Torr; nachfolgendes Behandeln mit Acetylen;
参考文献
Union Carbide and Carbon Res.Lab.
Patent: US2163720 , 1937 ;
反应条件
diethyl ether; potassium 2-methyl-2-butoxide
参考文献
Thompson; Burr; Shaw
Journal of the American Chemical Society, 1941 , vol. 63, p. 187
反应条件
potassium hydroxide
T=6°C; P=2574.3 Torr; solid form;
参考文献
Union Carbide and Carbon Res.Labor.
Patent: US2163720 , 1937 ;
反应条件
potassium hydroxide in tetrahydrofuran
参考文献
Kovalev,B.G. et al.
Journal of Organic Chemistry USSR (English Translation), 1975 , vol. 11, p. 1172 - 1175
Zhurnal Organicheskoi Khimii, 1975 , vol. 11, p. 1183 - 1187
参考文献
Union Carbide and Carbon Res.Labor.
Patent: US2175581 , 1937 ;
反应条件
Einleiten von Acetylen in die erhaltenen Natriumverbindung, unter Druck;
参考文献
Leers
Bulletin de la Societe Chimique de France, 1926 , vol. <4>39, p. 423
