反式-2-苯基-1-环已醇合成路线 （共 72 条）
反应条件
MS 4 Angstroem; (S)-1-methyl-2-[(dihydroisoindol-2-yl)methyl]pyrrolidine; tin(ll) chloride in dichloromethane 24 h; Ambient temperaturereactions under var. conditions and reactions of derivatives; Product distribution;
参考文献
Oriyama, Takeshi; Hori, Yoko; Imai, Keisuke; Sasaki, Ryosuke
Tetrahedron Letters, 1996 , vol. 37, # 47 p. 8543 - 8546
反应条件
(1S,4S)-4-Bn-1-nBu-AZADOH; sodium hydrogencarbonate in dichloromethane T=-40°C; 3 h; Resolution of racemateInert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Tomizawa, Masaki; Shibuya, Masatoshi; Iwabuchi, Yoshiharu
Organic Letters, 2009 , vol. 11, # 8 p. 1828 - 1831
反应条件
peracetic acid; 2,4-dimethylpentane-2,4-diol cyclic chromate in tetrachloromethane; dichloromethane T=0°C; 0.5 h;
参考文献
Sasano, Yusuke; Nishiyama, Tomohiro; Tomizawa, Masaki; Shibuya, Masatoshi; Iwabuchi, Yoshiharu
Heterocycles, 2013 , vol. 87, # 10 p. 2109 - 2118
反应条件
(1S,3R,4S,5R,7R)-N-hydroxy-4-benzyl-1-isopropyl-2-azaadamantane; sodium hydrogencarbonate in dichloromethane T=-40°C; 3 h; Resolution of racemateInert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Hamada, Shohei; Wada, Yoshiyuki; Sasamori, Takahiro; Tokitoh, Norihiro; Furura, Takumi; Kawabata, Takeo
Tetrahedron Letters, 2014 , vol. 55, # 11 p. 1943 - 1945
反应条件
(1S,4S)-4-Bn-1-nBu-AZADOH; sodium hydrogencarbonate in dichloromethane T=-40°C; 3 h; Resolution of racemateInert atmosphere; optical yield given as percent eeenantioselective reaction;
参考文献
Tomizawa, Masaki; Shibuya, Masatoshi; Iwabuchi, Yoshiharu
Organic Letters, 2009 , vol. 11, # 8 p. 1828 - 1831
反应条件
(-)-sparteine in acetonitrile electrolysis: 'H' type divided cell separated by membrane Nafion 117, NaClO4 as supporting electrolyte, TEMPO-modified grafite felt electrode, charge passed 1.17 F mol-1, electrolysis potential 0.60 V (vs. Ag/AgCl);
参考文献
Chemical Communications, , # 24 p. 2745 - 2746
反应条件
chromium(VI) oxide; acetic acid
参考文献
Cook; Hewett; Lawrence
Journal of the Chemical Society, 1936 , p. 71,76
参考文献
Cook; Hewett; Lawrence
Journal of the Chemical Society, 1936 , p. 71,76
参考文献
Price; Karabinos
Journal of the American Chemical Society, 1940 , vol. 62, p. 1159
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Eliel et al.
Journal of Organic Chemistry, 1957 , vol. 22, p. 1533,1538
Full Text Show Details
Schaeffer; Collins
Journal of the American Chemical Society, 1956 , vol. 78, p. 124,130
反应条件
1: pyridine / 0 °C 2: thiolacetic acid potassium salt / N,N-dimethyl-formamide 3: borane-THF / 0 °C View Scheme
参考文献
Younai, Ashkaan; Fettinger, James C.; Shaw, Jared T.
Tetrahedron, 2012 , vol. 68, # 22 p. 4320 - 4327
