反式-3-(乙酰氨基)-2-巴豆酸乙酯合成路线 (共 11 条)
反应条件
copper(l) iodide; caesium carbonate; N-methyl-2-(methylamino)ethylamine in tetrahydrofuran T=70°C; 6 h;
参考文献
Jiang, Lei; Job, Gabriel E.; Klapars, Artis; Buchwald, Stephen L.
Organic Letters, 2003 , vol. 5, # 20 p. 3667 - 3669
反应条件
pyridine in tetrahydrofuran Acetylation; 24 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 64, # 18 p. 6907 - 6910
反应条件
1: NH4OAc / methanol / 60 h / 20 °C 2: pyridine / tetrahydrofuran / 15 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 124, # 49 p. 14552 - 14553
反应条件
pyridine in tetrahydrofuran T=95°C; 12 h;
参考文献
Enthaler, Stephan; Erre, Giulia; Junge, Kathrin; Holz, Jens; Boerner, Armin; Alberico, Elisabetta; Nieddu, Ilenia; Gladiali, Serafino; Beller, Matthias
Organic Process Research and Development, 2007 , vol. 11, # 3 p. 568 - 577
反应条件
pyridine in diethyl ether 1.) 0 deg C, 0.5 h; 2.) reflux, 1 h;
参考文献
Bulletin des Societes Chimiques Belges, , vol. 90, # 1 p. 75 - 82
反应条件
pyridine in diethyl ether
参考文献
Journal of Organic Chemistry USSR (English Translation), , vol. 13, p. 1069 - 1074
Zhurnal Organicheskoi Khimii, , vol. 13, p. 1161 - 1168
反应条件
aluminium trichloride
参考文献
Journal of Organic Chemistry, , vol. 6, p. 70,74
反应条件
pyridine; diethyl ether
参考文献
Helvetica Chimica Acta, , vol. 33, p. 1787,1795
参考文献
Helvetica Chimica Acta, , vol. 33, p. 1787,1795
反应条件
hydrogen; palladium on activated charcoal in methanol
P=760.051 Torr; 16 h;
参考文献
Landert, Heidi; Spindler, Felix; Wyss, Adrian; Blaser, Hans-Ulrich; Pugin, Benoit; Ribourduoille, Yann; Gschwend, Bjoern; Ramalingam, Balamurugan; Pfaltz, Andreas
Angewandte Chemie - International Edition, 2010 , vol. 49, # 38 p. 6873 - 6876