1,3,5,7-四甲基环四硅氧烷合成路线 (共 19 条)
反应条件
water in toluene T=20°C; 27 h; hydrolytic copolycondensation depending on final concentration of hydrochloric acid; other dialkyldichlorosilanes; Product distribution;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 61, # 6.2 p. 1378 - 1383,1257 - 1261
反应条件
tetrahydrofuran; lithium T=35 - 45°C; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 7 p. 1528 - 1533,1358 - 1362
参考文献
Journal of the American Chemical Society, , vol. 68, p. 963
反应条件
sodium hydroxide in diethyl ether T=0 - 5°C;
参考文献
Martynova, T. N.; Korchkov, V. P.
Journal of Organometallic Chemistry, 1983 , vol. 248, # 3 p. 241 - 250
反应条件
platinum in toluene T=70°C; 3 h; regioselective reaction;
参考文献
Letters in Organic Chemistry, , vol. 8, # 5 p. 361 - 363
反应条件
water; sulphur(VI) hexafluoride P=30.002 Torr; Irradiationvar. time of irradiation; Product distributionMechanism;
参考文献
Pola, J.; Cukanova, D.; Ponec, R.; Stanczyk, W.
Journal of Organometallic Chemistry, 1994 , vol. 468, # 1-2 p. 49 - 54
反应条件
tris(pentafluorophenyl)-borane in benzene-d6 T=20°C; 20 h;
参考文献
Khalimon, Andrey Y.; Piers, Warren E.; Blackwell, James M.; Michalak, David J.; Parvez, Masood
Journal of the American Chemical Society, 2012 , vol. 134, # 23 p. 9601 - 9604
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene T=40°C; 3 h; Inert atmosphere; regioselective reaction;
参考文献
El Malki, Abdelghani; Hannioui, Abdellah; El Mostapha, Rakib; Knouzi, Nourredine; Vaultier, Michel
Letters in Organic Chemistry, 2011 , vol. 8, # 5 p. 361 - 363
反应条件
platinum-based catalyst in toluene T=80°C; 3 h; regioselective reaction;
参考文献
El Malki, Abdelghani; Hannioui, Abdellah; El Mostapha, Rakib; Knouzi, Nourredine; Vaultier, Michel
Letters in Organic Chemistry, 2011 , vol. 8, # 5 p. 361 - 363