2-羟基-5-氯甲基苯甲醛合成路线 （共 9 条）
反应条件
hydrogenchloride T=20°C;
参考文献
Razi, Syed S.; Ali, Rashid; Srivastava, Priyanka; Misra, Arvind
Tetrahedron Letters, 2014 , vol. 55, # 5 p. 1052 - 1056
反应条件
hydrogenchloride; formaldehyd in dichloromethane
参考文献
US5569677 A1, ;
US 5569677 A
反应条件
hydrogenchloride T=25 - 30°C;
参考文献
Chem. Zentralbl., , vol. 73, # II p. 894
DE114194 ;
Fortschr. Teerfarbenfabr. Verw. Industriezweige, vol. 6, p. 139
反应条件
hydrogenchloride T=20°C; 48 h;
参考文献
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, , vol. 58, # 7 p. 1411 - 1424
反应条件
1: magnesium chloride; triethylamine / acetonitrile / 20 °C 2: hydrogenchloride; zinc(II) chloride / water / 24 h / 20 °C View Scheme
参考文献
European Journal of Medicinal Chemistry, , vol. 75, p. 31 - 42
参考文献
Tanaka, Tomohide; Tsurutani, Keiko; Komatsu, Atsushi; Ito, Toyofumi; Iida, Kazumi; Fujii, Yuki; Nakano, Yoshiharu; Usui, Yoshiharu; Fukuda, Yutaka; Chikira, Makoto
Bulletin of the Chemical Society of Japan, 1997 , vol. 70, # 3 p. 615 - 629
反应条件
1: With 1,3,5,7-tetra-azatricyclo[5.1.1.13,5]decane; acetic acid in water Sommelet reaction; 1 h; Reflux; 2: With hydrogenchloride; water Sommelet reaction; 0.0833333 h; Reflux;
参考文献
Mei, Fu-Ming; Chen, Li-Juan; Li, Guang-Xing
Applied Organometallic Chemistry, 2010 , vol. 24, # 2 p. 86 - 91
反应条件
nitric acid; acetic acid
T=30 - 40°C;
参考文献
Tang, Rui-Ren; Huang, Ke-Long; Tang, Zi-Long; Yang, Qing
Synthetic Communications, 2007 , vol. 37, # 8 p. 1347 - 1354
反应条件
1: benzene / 1 h / Heating
2: aq. NaOH / 2 h
View Scheme
参考文献
El-Sonbati; El-Bindary; Rashed
Spectrochimica Acta - Part A: Molecular and Biomolecular Spectroscopy, 2002 , vol. 58, # 7 p. 1411 - 1424
