1-N-乙基苯-1,2-二胺合成路线 （共 25 条）
反应条件
hydrogen; palladium 10 on activated carbon in ethanol P=2585.81 Torr; 2 h; Product distribution / selectivity;
参考文献
ASTRAZENECA AB; ASTRAZENECA UK LIMITED
Patent: WO2008/56150 A1, 2008 ;
Location in patent: Page/Page column 126 ;
WO 2008/056150 A1
反应条件
ethylenediamine in ethanol T=20°C; 0.25 h;
参考文献
Ilangovan, Andivelu; Kumar, Rajendran Ganesh
Chemistry - A European Journal, 2010 , vol. 16, # 9 p. 2938 - 2943
反应条件
palladium 10 on activated carbon in toluene T=170°C; 1.5 h; Microwave irradiationInert atmosphere;
参考文献
De Luca, Lidia; Porcheddu, Andrea
European Journal of Organic Chemistry, 2011 , # 29 p. 5791 - 5795
反应条件
zeolite NaY 12 h; Heating;
参考文献
Ebenezer, Warren J.; Hutchings, Michael G.; Jones, Ken; Lambert, David A.; Watt, Ian
Tetrahedron Letters, 2007 , vol. 48, # 9 p. 1641 - 1643
反应条件
1: 50 percent / H2 / 10percent Pd/C / ethanol 2: 40 percent / NH2OH*HCl, NaOAc / aq. ethanol / Ambient temperature View Scheme
参考文献
Essassi, El Mokhtar; Salem, Moussa; Viallefont, Philippe
Bulletin de la Societe Chimique de France, 1987 , # 5 p. 890 - 892
反应条件
hydroxylamine hydrochloride; sodium acetate in ethanol Ambient temperature;
参考文献
Essassi, El Mokhtar; Salem, Moussa; Viallefont, Philippe
Bulletin de la Societe Chimique de France, 1987 , # 5 p. 890 - 892
反应条件
1: ethanol / 170 °C 2: tin (II)-chloride; aqueous hydrochloric acid View Scheme
参考文献
Weidenhagen; Train
Chemische Berichte, 1942 , vol. 75, p. 1936,1942
参考文献
Amos,D.; Gillis,R.G.
Australian Journal of Chemistry, 1969 , vol. 22, p. 1555 - 1556
反应条件
Pt-TiO2 T=32°C; 4 h; UV-irradiationInert atmosphere;
参考文献
Selvam; Swaminathan
Tetrahedron Letters, 2011 , vol. 52, # 26 p. 3386 - 3392
参考文献
Hinsberg; Funcke
Chemische Berichte, 1894 , vol. 27, p. 2188
