(9H-芴-9-基)-癸基(2-氧代乙基)氨基甲酸甲酯合成路线 （共 7 条）
反应条件
sulfuric acid; triethylamine in n-heptane; dichloromethane; water; dimethyl sulfoxide
参考文献
US2003/45457 A1, ;
US2003/69391 A1, ;
反应条件
formic acid T=20°C; 4 h;
参考文献
WO2011/5959 A1, ;
Page/Page column 23-24 ;
反应条件
1.1: butan-1-ol; water / 60 °C 2.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 16 h / 50 °C 3.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C 3.2: 0.92 h / 0 - 5 °C 4.1: formic acid / 4 h / 20 °C View Scheme
反应条件
1.1: butan-1-ol / 60 °C 2.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 48 h / 50 °C / 2280.15 Torr 3.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C 3.2: 0.92 h / 0 - 5 °C 4.1: formic acid / 4 h / 20 °C View Scheme
反应条件
1.1: hydrogen / platinum on activated charcoal / butan-1-ol; water / 16 h / 50 °C 2.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C 2.2: 0.92 h / 0 - 5 °C 3.1: formic acid / 4 h / 20 °C View Scheme
反应条件
1.1: sodium hydroxide / toluene; water / 0.08 - 0.17 h / 0 - 5 °C 1.2: 0.92 h / 0 - 5 °C 2.1: formic acid / 4 h / 20 °C View Scheme
反应条件
1: sodium hydroxide / toluene; water / 1.17 h / 0 - 5 °C 2: formic acid / 4 h / 20 °C View Scheme
