1-(苄氧基)-2-(氯甲基)苯合成路线 （共 10 条）
反应条件
2,4,6-trichloro-1,3,5-triazine; dimethyl sulfoxide T=20°C; 0.166667 h; chemoselective reaction;
参考文献
Sun, Lili; Peng, Guisheng; Niu, Hongmei; Wang, Qiang; Li, Chunbao
Synthesis, 2008 , # 24 art. no. F17308SS, p. 3919 - 3924
反应条件
1: 94 percent / potassium carbonate / acetone / 4 h / Heating 2: 92 percent / thionyl chloride / CH2Cl2 / 3 h / 0 °C View Scheme
参考文献
Moridani, Majid Y.; Tilbrook, Gary S.; Khodr, Hicham H.; Hider, Robert C.
Journal of Pharmacy and Pharmacology, 2002 , vol. 54, # 3 p. 349 - 364
反应条件
1: 94 percent / potassium carbonate / acetone / 4 h / Heating 2: 92 percent / thionyl chloride / CH2Cl2 / 3 h / 0 °C View Scheme
参考文献
Lisowski, Vincent; Enguehard, Cecile; Lancelot, Jean-Charles; Caignard, Daniel-Henri; Lambel, Stephanie; Leonce, Stephane; Pierre, Alain; Atassi, Ghanem; Renard, Pierre; Rault, Sylvain
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 16 p. 2205 - 2208
反应条件
1: K2CO3 / methanol / Heating 2: NaBH4 / methanol / 20 °C 3: SOCl2 / dioxane / 20 °C View Scheme
参考文献
Lisowski, Vincent; Enguehard, Cecile; Lancelot, Jean-Charles; Caignard, Daniel-Henri; Lambel, Stephanie; Leonce, Stephane; Pierre, Alain; Atassi, Ghanem; Renard, Pierre; Rault, Sylvain
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 16 p. 2205 - 2208
反应条件
1: NaBH4 / methanol / 20 °C 2: SOCl2 / dioxane / 20 °C View Scheme
参考文献
Lisowski, Vincent; Enguehard, Cecile; Lancelot, Jean-Charles; Caignard, Daniel-Henri; Lambel, Stephanie; Leonce, Stephane; Pierre, Alain; Atassi, Ghanem; Renard, Pierre; Rault, Sylvain
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 16 p. 2205 - 2208
反应条件
in N,N-dimethyl-formamide T=100°C; 2 h;
参考文献
Lee, Jeewoo; Lee, Ju-Hyun; Kim, Su Yeon; Perry, Nicholas A.; Lewin, Nancy E.; Ayres, Jolene A.; Blumberg, Peter M.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2022 - 2031
反应条件
in acetonitrile T=20°C;
参考文献
Lisowski, Vincent; Enguehard, Cecile; Lancelot, Jean-Charles; Caignard, Daniel-Henri; Lambel, Stephanie; Leonce, Stephane; Pierre, Alain; Atassi, Ghanem; Renard, Pierre; Rault, Sylvain
Bioorganic and Medicinal Chemistry Letters, 2001 , vol. 11, # 16 p. 2205 - 2208
反应条件
dihydrogen peroxide; vanadium pentoxide; Aliquatreg; 336 in water 6 h; Heating;
参考文献
Li, Chunbao; Zheng, Pengwu; Li, Jie; Zhang, Hang; Cui, Yi; Shao, Qiyun; Ji, Xiujie; Zhang, Jian; Zhao, Pengying; Xu, Yanli
Angewandte Chemie - International Edition, 2003 , vol. 42, # 41 p. 5063 - 5066
反应条件
1: 96 percent / dimethylformamide / 2 h / 100 °C 2: 97 percent / NaOH / H2O / Heating View Scheme
参考文献
Lee, Jeewoo; Lee, Ju-Hyun; Kim, Su Yeon; Perry, Nicholas A.; Lewin, Nancy E.; Ayres, Jolene A.; Blumberg, Peter M.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2022 - 2031
反应条件
1: 96 percent / dimethylformamide / 2 h / 100 °C
2: 97 percent / NaOH / H2O / Heating
3: 90 percent / H2SO4 / 2 h / Heating
View Scheme
参考文献
Lee, Jeewoo; Lee, Ju-Hyun; Kim, Su Yeon; Perry, Nicholas A.; Lewin, Nancy E.; Ayres, Jolene A.; Blumberg, Peter M.
Bioorganic and Medicinal Chemistry, 2006 , vol. 14, # 6 p. 2022 - 2031
