1,3-二氯-1,1,3,3,-四甲基二硅氧烷合成路线 (共 57 条)
反应条件
meta-chloroperoxybenzoic acid in benzene T=25°C; ΔH(excit.), ΔG(excit.), ΔS(excit.); Rate constantThermodynamic dataMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 59, # 1.2 p. 151 - 157,130 - 135
反应条件
tris(1,3-divinyl-1,1,3,3-tetramethyldisiloxane)-bis-platinum(0) in toluene Heating;
参考文献
Journal of Organometallic Chemistry, , vol. 690, # 20 SPEC. ISS. p. 4478 - 4487
反应条件
aluminium trichloride in neat (no solvent) ((CH3)2SiO)4 and AlCl3 at about 120°C;;
参考文献
US2645654 , ;
C. A., , p. 7050
反应条件
1,4-dioxane; lithium T=65°C; 7 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 7 p. 1528 - 1533,1358 - 1362
反应条件
1,4-dioxane; lithium T=65°C; 7 h; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 7 p. 1528 - 1533,1358 - 1362
反应条件
sodium nitrate T=0°C; 2 h; Yield givenFurther byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Russian Journal of General Chemistry, , vol. 68, # 4 p. 658 - 659
Zhurnal Obshchei Khimii, , vol. 68, # 4 p. 699 - 700
反应条件
hydrogenchloride in 1,4-dioxane; benzene T=29.9°C; without added water; Rate constant;
参考文献
Journal of Organometallic Chemistry, , vol. 356, p. 141 - 150
参考文献
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , p. 806,807, 809; engl. Ausg. S. 827, 828, 830
反应条件
in hexane T=20°C; Rate constant;
参考文献
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), , vol. 34, # 10 p. 2010 - 2013
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, , # 10 p. 2177 - 2180
反应条件
1,4-dioxane; lithium T=65°C; 7 h; other temperature; Product distributionMechanism;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 55, # 7 p. 1528 - 1533,1358 - 1362