2,2,6-三甲基环己酮合成路线 （共 96 条）
反应条件
hydrogen; palladium on activated charcoal
参考文献
Helvetica Chimica Acta, , vol. 68, p. 1961 - 1985
反应条件
sodium hydroxide in methanol Ambient temperature;
参考文献
Helvetica Chimica Acta, , vol. 57, p. 1098 - 1116
反应条件
manganese bromide tetrahydrate; methyllithium T=22°C; 3 h;
参考文献
Tetrahedron Letters, , vol. 34, # 46 p. 7395 - 7398
反应条件
1: 89 percent / py 2: 89 percent / Jones reagent / acetone / 10 h / ice cooling 3: 4 percent / NaOH / methanol; H2O / 72 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 113, # 5 p. 1907 - 1920
反应条件
1: 89 percent / Jones reagent / acetone / 10 h / ice cooling 2: 4 percent / NaOH / methanol; H2O / 72 h / Heating View Scheme
参考文献
Chemische Berichte, , vol. 113, # 5 p. 1907 - 1920
反应条件
1: CH3COCl 3: CH3I; MgBr2 / ethylene glycol dimethyl ether View Scheme
参考文献
Sn: Org.Comp.12, 1.4.1.1.1.5.2.2, page 97 - 113
反应条件
2: CH3I; MgBr2 / ethylene glycol dimethyl ether View Scheme
参考文献
Sn: Org.Comp.12, 1.4.1.1.1.5.2.2, page 97 - 113
反应条件
(i) Li, liq. NH3, H2O, Et2O, (ii) /BRN= 969135/; Multistep reaction;
参考文献
Journal of the American Chemical Society, , vol. 93, p. 1027 - 1029
反应条件
lithium diisopropyl amide 1) THF, a) -78 deg C, 1 h, b) 0 deg C, 1 h, 2) 0 deg C, 20 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 7 p. 2094 - 2114
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine in dichloromethane 78 h; Ambient temperature; Yield given. Yields of byproduct given;
参考文献
Canadian Journal of Chemistry, , vol. 70, # 7 p. 2094 - 2114
