N-叔丁基羰基-4-溴苯胺合成路线 （共 9 条）
反应条件
N-ethyl-N,N-diisopropylamine in N,N-dimethyl-formamide
T=25°C; 2 h;
参考文献
Sasaki, Kaname; Crich, David
Organic Letters, 2011 , vol. 13, # 9 p. 2256 - 2259
反应条件
sodium hydroxide in hexane
参考文献
Wella Aktiengesellschaft
Patent: US6500213 B1, 2002 ;
反应条件
triethylamine in ethyl acetate
T=80°C; Inert atmosphereSealed tube;
参考文献
Cai, Shangjun; Chen, Chao; Sun, Zelin; Xi, Chanjuan
Chemical Communications, 2013 , vol. 49, # 40 p. 4552 - 4554
反应条件
sodium hydroxide in tert-butyl methyl ether; water
T=0 - 25°C; 4.5 h;
参考文献
Zhu, Lingjian; Miao, Zhenyuan; Sheng, Chunquan; Guo, Wei; Yao, Jianzhong; Liu, Wenfeng; Che, Xiaoying; Wang, Wenya; Cheng, Pengfei; Zhang, Wannian
European Journal of Medicinal Chemistry, 2010 , vol. 45, # 7 p. 2726 - 2732
反应条件
thionyl chloride
und anschliessend mit 4-Brom-anilin in Chloroform;
参考文献
Degnan; Shoemaker
Journal of the American Chemical Society, 1946 , vol. 68, p. 104
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Bryant; Mitchell
Journal of the American Chemical Society, 1938 , vol. 60, p. 2748,2750
反应条件
1: 94 percent / Et3N / diethyl ether / 18 h / Ambient temperature
2: 1.) MeLi, 2.) n-BuLi
View Scheme
参考文献
Stanetty, Peter; Krumpak, Barbara; Rodler, Inge K.
Journal of Chemical Research, Miniprint, 1995 , # 9 p. 2111 - 2122
反应条件
1: 94 percent / Et3N / diethyl ether / 18 h / Ambient temperature
2: 1.) MeLi, 2.) n-BuLi
View Scheme
参考文献
Stanetty, Peter; Krumpak, Barbara; Rodler, Inge K.
Journal of Chemical Research, Miniprint, 1995 , # 9 p. 2111 - 2122
参考文献
Dewar; Scott
Journal of the Chemical Society, 1957 , p. 1445
反应条件
n-butyllithium; methyllithium
Yield given. Multistep reaction;
参考文献
Stanetty, Peter; Krumpak, Barbara; Rodler, Inge K.
Journal of Chemical Research, Miniprint, 1995 , # 9 p. 2111 - 2122
