5-氯-3-苯基-1H-吲哚-2-甲腈合成路线 （共 3 条）
反应条件
in dimethyl sulfoxide T=140°C; 2 h;
参考文献
Garanti, Luisa; Zecchi, Gaetano
Journal of Organic Chemistry, 1980 , vol. 45, # 23 p. 4767 - 4769
反应条件
1: 1) sodium hydride / 1) DMF, ice cooling, 2) 16 h, room temperature 2: 1) aqu. sodium nitrite, 2) sodium azide / 1) 1N aqueous hydrochloric acid, ice cooling, 2) pH 5, 30 min 3: 31 percent / dimethylsulfoxide / 2 h / 140 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4767 - 4769
反应条件
1: 1) aqu. sodium nitrite, 2) sodium azide / 1) 1N aqueous hydrochloric acid, ice cooling, 2) pH 5, 30 min 2: 31 percent / dimethylsulfoxide / 2 h / 140 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 45, # 23 p. 4767 - 4769
