(2,2-二氯环丙基)苯合成路线 （共 37 条）
反应条件
aluminium trichloride in tetrachloromethane T=10 - 15°C; 6 h;
参考文献
Tishchenko, I. G.; Kulinkovich, O. G.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, p. 268 - 271
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 2 p. 303 - 308
反应条件
1.1: reduction 2.1: nitrosyl chloride / CH2Cl2; liquid sulphur dioxide / 5 h / -55 °C 2.2: CDCl3 / 1461 h / -20 °C View Scheme
参考文献
Bondarenko; Gavrilova; Kazantseva; Tikhanushkina; Nifant'ev; Saginova; Zyk
Russian Journal of Organic Chemistry, 2006 , vol. 42, # 2 p. 249 - 255
反应条件
1.1: reduction 2.1: nitrosyl chloride / CH2Cl2; liquid sulphur dioxide / 5 h / -55 °C 2.2: 12 percent / sodium carbonate / H2O / 0 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 42, # 2 p. 249 - 255
反应条件
samarium diiodide; thiophenol in tetrahydrofuran Ambient temperatureIrradiation;
参考文献
Ogawa, Akiya; Ohya, Syoji; Hirao, Toshikazu
Chemistry Letters, 1997 , # 3 p. 275 - 276
反应条件
samarium diiodide in tetrahydrofuran T=25°C; 8 h; Irradiation;
参考文献
Chemistry Letters, , # 3 p. 275 - 276
反应条件
diisobutylaluminium hydride; bis(cyclopentadienyl)titanium dichloride in 1,4-dioxane T=75°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Dzhemilev, U. M.; Gaisin, R. L.; Turchin, A. A.; Khalikova, N. R.; Baikova, I. P.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1990 , vol. 39, # 5.2 p. 967 - 974
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1990 , # 5 p. 1080 - 1087
反应条件
lithium aluminium tetrahydride; Zr(acac)4 in 1,4-dioxane T=75°C; 6 h;
参考文献
Dzhemilev, U. M.; Gaisin, R. L.; Turchin, A. A.; Tolstikov, G. A.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1991 , vol. 40, # 9.2 p. 1845 - 1848
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1991 , # 9 p. 2084 - 2087
反应条件
lithium aluminium tetrahydride in diethyl ether T=0°C; 8 h; Irradiation; Yield given. Title compound not separated from byproducts;
参考文献
Shimizu, Nobujiro; Watanabe, Kenji; Tsuno, Yuho
Bulletin of the Chemical Society of Japan, 1984 , vol. 57, # 3 p. 885 - 886
反应条件
sodium tetrahydroborate; CaO; Rh-complex other complexes, activity of complexes, rate of reaction W0; Product distribution;
参考文献
Dovganyuk, V. F.; Sharf, V. Z.; Saginova, L. G.; Antokol'skaya, I. I.; Bol'shakova, L. I.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1989 , vol. 38, # 4 p. 699 - 703
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1989 , # 4 p. 777 - 782
反应条件
NOCl*2SO3 in dichloromethane T=20°C; 0.5 h;
参考文献
Bondarenko; Gavrilova; Murodov; Zefirov; Zyk
Russian Journal of Organic Chemistry, 2013 , vol. 49, # 2 p. 186 - 194
Zh. Org. Khim., 2013 , vol. 49, # 2 p. 198 - 206,9
