1-(4,5-二甲氧基-2-甲基苯基)乙酮合成路线 （共 19 条）
参考文献
Harding; Weizmann
Journal of the Chemical Society, 1910 , vol. 97, p. 1128
参考文献
Harding; Weizmann
Journal of the Chemical Society, 1910 , vol. 97, p. 1128
参考文献
Harding; Weizmann
Journal of the Chemical Society, 1910 , vol. 97, p. 1128
反应条件
1: aq. K2CO3, KMnO4 2: aq. AcOH, Pb(OAc)4 View Scheme
参考文献
Hatam,N.A.R.; Whiting,D.A.
Journal of the Chemical Society [Section] C: Organic, 1969 , p. 1921 - 1932
反应条件
AlCl3, aluminium chloride in carbon disulfide
T=0 - 20°C; Inert atmosphere;
参考文献
Solomek, Tomas; Stacko, Peter; Tazhe Veetil, Aneesh; Pospisil, Tomas; Klan, Petr
Journal of Organic Chemistry, 2010 , vol. 75, # 21 p. 7300 - 7309
反应条件
lithium perchlorate
T=60°C; Friedel Crafts acylation; 1 h;
参考文献
Kim, Joa Kyum; Kim, Young Ha; Nam, Ho Tae; Kim, Bum Tae; Heo, Jung-Nyoung
Organic Letters, 2008 , vol. 10, # 16 p. 3543 - 3546
反应条件
in isopropyl alcohol
15 h; IrradiationInert atmosphere;
参考文献
Tazhe Veetil, Aneesh; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Pavlikova, Nela; Heger, Dominik; Klan, Petr
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8232 - 8242
反应条件
1.1: sodium iodide / acetone / 0.17 h / 20 °C
1.2: 20 °C
2.1: isopropyl alcohol / 15 h / Irradiation; Inert atmosphere
View Scheme
参考文献
Tazhe Veetil, Aneesh; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Pavlikova, Nela; Heger, Dominik; Klan, Petr
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8232 - 8242
反应条件
in acetonitrile
15 h; IrradiationInert atmosphere;
参考文献
Tazhe Veetil, Aneesh; Solomek, Tomas; Ngoy, Bokolombe Pitchou; Pavlikova, Nela; Heger, Dominik; Klan, Petr
Journal of Organic Chemistry, 2011 , vol. 76, # 20 p. 8232 - 8242
反应条件
1: aqueous-methanolic KOH-solution
2: aluminium chloride; carbon disulfide / in der Kaelte und nachfolgendem Erwaermen auf dem Wasserbad
View Scheme
参考文献
Fargher; Perkin
Journal of the Chemical Society, 1921 , vol. 119, p. 1732
