甲基N-[(苄氧基)羰基]-L-缬氨酸酯合成路线 （共 35 条）
反应条件
4-(N,N-dimethlyamino)pyridine 1) CH2CN, 25 deg C, 10 min, 2) CH3CN, 82 deg C, 36 h; Yield given. Multistep reaction;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias
Synlett, 1997 , vol. 1997, # 8 p. 925 - 928
反应条件
4-(N,N-dimethlyamino)pyridine 1) CH3CN, 82 deg C, 3 h, 2) CH3CN, 25 deg C, 10 min, 3) CH3CN, 82 deg C, 37 h; Yield given. Multistep reaction;
参考文献
Knoelker, Hans-Joachim; Braxmeier, Tobias
Synlett, 1997 , vol. 1997, # 8 p. 925 - 928
反应条件
bis(2-pyridinyl)-disulfide; dichloromethane; triphenylphosphine
参考文献
Sankyo Co.
Patent: DE2057718 , 1970 ;
参考文献
Synge
Biochemical Journal, 1948 , vol. 42, p. 99,101
参考文献
Miyoshi,M.
Bulletin of the Chemical Society of Japan, 1970 , vol. 43, # 10 p. 3321
反应条件
1: acetic acid tert-butyl ester With lithium diisopropyl amide in tetrahydrofuran; n-heptane; ethylbenzene T=-50°C; 2: methyl (2S)-3-methyl-[(benzyloxy)carbonylamino]butanoate in tetrahydrofuran; n-heptane; ethylbenzene T=-55°C; cross-Claisen condensation;
参考文献
Honda, Yutaka; Katayama, Satoshi; Kojima, Mitsuhiko; Suzuki, Takayuki; Izawa, Kunisuke
Tetrahedron Letters, 2003 , vol. 44, # 15 p. 3163 - 3166
反应条件
sodium hydroxide; sodium tetrahydroborate 1) EtOH, RT, 14h, 2) MeOH, 2.5h; Yield given. Multistep reaction;
参考文献
Nakano, Masato; Atsuumi, Shugo; Koike, Yutaka; Tanaka, Seiichi; Funabashi, Hiroshi; et al.
Chemistry Letters, 1990 , # 4 p. 505 - 508
反应条件
triethylsilane; palladium on activated charcoal in methanol 0.833333 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 17 p. 6599 - 6601
反应条件
2C33H37N*H2O7S2; water T=80°C; 9 h; optical yield given as percent ee;
参考文献
Koshikari, Yoshiki; Sakakura, Akira; Ishihara, Kazuaki
Organic Letters, 2012 , vol. 14, # 12 p. 3194 - 3197
参考文献
Photaki; Yiotakis
Journal of the Chemical Society. Perkin transactions 1, 1976 , # 3 p. 259 - 264
