(R)-(-)-1-苯乙基 硫代异氰酸酯合成路线 （共 28 条）
反应条件
1: With potassium carbonate in water T=20°C; 1 h; Inert atmosphere; 2: With 2,4,6-trichloro-1,3,5-triazine in dichloromethane; water T=0°C; 0.5 h; Inert atmosphere; 3: With sodium hydroxide in dichloromethane; water pH=11; Inert atmosphere;
参考文献
Sun, Nan; Li, Bin; Shao, Jianping; Mo, Weimin; Hu, Baoxiang; Shen, Zhenlu; Hu, Xinquan
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 61 - 70
反应条件
1: Ammonium thiocyanate With selectfluor in acetonitrile T=20°C; 0.333333 h; 2: sec-phenethyl alcohol in acetonitrile 0.5 h;
参考文献
Journal of Fluorine Chemistry, , vol. 137, p. 123 - 125
反应条件
iodine; oxalic acid in nitromethane T=60°C; 2 h;
参考文献
Miyake, Hideyoshi; Nakao, Yuichi; Sasaki, Mitsuru
Chemistry Letters, 2006 , vol. 35, # 11 p. 1262 - 1263
反应条件
in acetonitrile T=60°C; 3.5 h;
参考文献
Tetrahedron Letters, , vol. 53, # 5 p. 491 - 493
参考文献
Journal of the American Chemical Society, , vol. 78, p. 4965
反应条件
sodium hydroxide dann mit Chlorokohlensaeure-aethylester;
参考文献
Journal of the American Chemical Society, , vol. 78, p. 4965
Journal of the Indian Chemical Society, , vol. 35, p. 657,658
反应条件
T=60°C; Neat (no solvent);
参考文献
Tetrahedron Letters, , vol. 50, # 1 p. 32 - 34
反应条件
T=60°C; Neat (no solvent);
参考文献
Tetrahedron Letters, , vol. 50, # 1 p. 32 - 34
反应条件
pyridine in dichloromethane T=50°C; 0.183333 h; Microwave irradiation; Overall yield = 83 percent; chemoselective reaction;
参考文献
Synthetic Communications, , vol. 43, # 8 p. 1138 - 1144
反应条件
1: HCl, Oxone / dimethylformamide / Ambient temperature 2: triethylamine / tetrahydrofuran / Ambient temperature View Scheme
参考文献
Tetrahedron Letters, , vol. 38, # 9 p. 1597 - 1598
