苯并[b]萘并[2,3-d]呋喃合成路线 （共 32 条）
反应条件
1: 84 percent / potassium carbonate / N,N-dimethyl-acetamide / 2 h / Heating 2: m-chloroperbenzoic acid / CHCl3 / 6 h / 30 °C 3: 2.73 g / hydrochloric acid aq / methanol / 1 h / 20 °C 4: 100 percent / 2,6-lutidine / CH2Cl2 / 1 h / -30 °C 5: 80 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; bis(triphenylphosphine)palladium(II) chloride / dimethylformamide / 145 °C View Scheme
参考文献
Tetrahedron, , vol. 58, # 29 p. 5927 - 5931
反应条件
1: 84 percent / potassium carbonate / N,N-dimethyl-acetamide / 2 h / Heating 2: m-chloroperbenzoic acid / CHCl3 / 6 h / 30 °C 3: 2.73 g / hydrochloric acid aq / methanol / 1 h / 20 °C 4: 100 percent / 2,6-lutidine / CH2Cl2 / 1 h / -30 °C 5: 80 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; bis(triphenylphosphine)palladium(II) chloride / dimethylformamide / 145 °C View Scheme
参考文献
Tetrahedron, , vol. 58, # 29 p. 5927 - 5931
反应条件
1: m-chloroperbenzoic acid / CHCl3 / 6 h / 30 °C 2: 2.73 g / hydrochloric acid aq / methanol / 1 h / 20 °C 3: 100 percent / 2,6-lutidine / CH2Cl2 / 1 h / -30 °C 4: 80 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene; lithium chloride; bis(triphenylphosphine)palladium(II) chloride / dimethylformamide / 145 °C View Scheme
参考文献
Tetrahedron, , vol. 58, # 29 p. 5927 - 5931
反应条件
1: 61 percent / 1 h / 280 - 285 °C 2: 84 percent / S / tetrahydrothiophene 1,1-dioxide / 1 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 33, # 1 p. 109 - 111
反应条件
1: 61 percent / 1 h / 280 - 285 °C 2: 84 percent / S / tetrahydrothiophene 1,1-dioxide / 1 h / Heating View Scheme
参考文献
Journal of Heterocyclic Chemistry, , vol. 33, # 1 p. 109 - 111
反应条件
1.1: N,N,N',N,-tetramethylethylenediamine; n-butyllithium / tetrahydrofuran; hexane / 3 h / -78 - 20 °C / |Inert atmosphere 1.2: 12 h / 20 °C / |Inert atmosphere 2.1: ammonium chloride / water 3.1: palladium diacetate; potassium carbonate; iodine / acetonitrile / 12 h / 20 - 80 °C / |Schlenk technique; |Inert atmosphere; |Sealed tube View Scheme
参考文献
Advanced Synthesis and Catalysis, , vol. 355, # 18 p. 3625 - 3632
反应条件
1: 4-(N,N-dimethlyamino)pyridine; triethylamine / dichloromethane / 15 h / 20 °C / |Schlenk technique; |Inert atmosphere 2: [Ni0(1,5-cyclooctadiene)2]; dcype; caesium carbonate / anhydrous xylene / 72 h / 160 °C View Scheme
参考文献
Tetrahedron, , vol. 69, # 27-28 p. 5780 - 5790
反应条件
hydrogen bromide; acetic acid
参考文献
Journal of the Indian Chemical Society, , vol. 34, p. 155,157
参考文献
Journal of the Indian Chemical Society, , vol. 31, p. 101,106
反应条件
T=490°C; Leiten ueber einen Chromoxyd-Aluminiumoxyd-Katalysator;
参考文献
Journal of the American Chemical Society, , vol. 70, p. 1245
