(R,R)-(-)-2,3-丁二醇合成路线 (共 64 条)
反应条件
hydrogen; Pt/Al2O3; cinchonine in toluene P=80256.4 Torr; 1.91667 h; Further byproducts given. Yields of byproduct given;
参考文献
Studer, Martin; Okafor, Victor; Blaser, Hans-Ulrich
Chemical Communications, 1998 , # 9 p. 1053 - 1054
反应条件
hydrogen; Pt/Al2O3; cinchonine in toluene P=80256.4 Torr; 1.91667 h; Yield given. Further byproducts given. Title compound not separated from byproducts;
参考文献
Studer, Martin; Okafor, Victor; Blaser, Hans-Ulrich
Chemical Communications, 1998 , # 9 p. 1053 - 1054
反应条件
recombinant human aldo-keto reductase AKR1B10; NADPH in aq. phosphate buffer T=25°C; pH=7; Enzymatic reaction; Reagent/catalyst; stereospecific reaction;
参考文献
Chemico-Biological Interactions, , vol. 202, # 1-3 p. 195 - 203
反应条件
1: With trimethylsilyl iodide in chloroform T=35°C; 12 h; 2: With methanol T=20°C; 2 h;
参考文献
Murali, Dhanabalan; Singaram, Bakthan; Brown, Herbert C.
Tetrahedron Asymmetry, 2000 , vol. 11, # 24 p. 4831 - 4834
反应条件
hydrogen; Pt/Al2O3; cinchonine in toluene P=80256.4 Torr; 1.91667 h; different reaction times; Rate constantProduct distribution;
参考文献
Studer, Martin; Okafor, Victor; Blaser, Hans-Ulrich
Chemical Communications, 1998 , # 9 p. 1053 - 1054
反应条件
E. coli JCL260 expressinig Thermoanaerobacter brockii adh T=30°C; pH=7; 48 h; Enzymatic reaction; enantioselective reaction;
参考文献
Yan, Yajun; Lee, Chia-Chi; Liao, James C.
Organic and Biomolecular Chemistry, 2009 , vol. 7, # 19 p. 3914 - 3917
反应条件
immobilised C. antarctica lipase B in phosphate buffer; decane; hexane 5 h;
参考文献
Liu, Rong; Hoegberg, Hans-Erik
Tetrahedron Asymmetry, 2001 , vol. 12, # 5 p. 771 - 778
反应条件
D-glucose in water T=33°C; 2 h; Microbiological reaction; optical yield given as percent eestereoselective reaction;
参考文献
Monsalve, Leandro N.; Cerrutti, Patricia; Galvagno, Miguel A.; Baldessari, Alicia
Biocatalysis and Biotransformation, 2010 , vol. 28, # 2 p. 137 - 143
反应条件
potassium phosphate buffer T=35°C; 13 h; Rhodotorula glutinis; Title compound not separated from byproducts;
参考文献
Tetrahedron Asymmetry, , vol. 8, # 4 p. 639 - 647
反应条件
L-(+)-tartaric acid beim Hydratisieren;
参考文献
Journal of the American Chemical Society, , vol. 58, p. 2399