2,4,6-三溴间苯二酚合成路线 (共 36 条)
反应条件
sodium hydroxide; sodium sulfite in methanol; water T=25°C; 0.25 h;
参考文献
Kiehlmann, E.; Lauener, R. W.
Canadian Journal of Chemistry, 1989 , vol. 67, p. 335 - 344
参考文献
Davis; Harrington
Journal of the American Chemical Society, 1934 , vol. 56, p. 129,131
反应条件
1: 30.7 g / NoOH; Na2SO3 / methanol; H2O / 0.25 h / 20 °C 2: 93 percent / K2CO3; KI / dimethylformamide / 16 h / 60 °C 3: nBuLi / tetrahydrofuran; hexane / -78 °C 4: 1.91 g / H2O 5: 92 percent / aq. Ba(OH)2 / Pd(PPh3)4 / 1,2-dimethoxy-ethane / 16 h / Heating View Scheme
参考文献
Luening, Ulrich; Abbass, Michael; Fahrenkrug, Frank
European Journal of Organic Chemistry, 2002 , # 19 p. 3294 - 3303
参考文献
Kohn; Steiner
Journal of Organic Chemistry, 1947 , vol. 12, p. 30,32
参考文献
Kohn; Steiner
Journal of Organic Chemistry, 1947 , vol. 12, p. 30,32
反应条件
potassium hydroxide; Raney Ni-Al alloy in water
T=90°C; 6 h;
参考文献
Liu, Guo-Bin; Zhao, Hong-Yun; Zhang, Jie; Thiemannb, Thies
Journal of Chemical Research, 2009 , # 6 p. 342 - 344