反应条件
1: decanoic acid methyl ester With diisobutylaluminium hydride in diethyl ether; hexane
T=-78°C; Reduction;
2: C42H38P2 in tetrahydrofuran; diethyl ether; hexane
T=-78 - 20°C; Wittig reaction;
3: acrolein in tetrahydrofuran; diethyl ether; hexane
T=-78 - 20°C; Wittig reaction; 0.5 h; Further stages.;
参考文献
Pohnert, Georg; Boland, Wilhelm
European Journal of Organic Chemistry, 2000 , # 9 p. 1821 - 1826