1,1-二甲基-2-丙烯基乙酸酯合成路线 （共 69 条）
反应条件
[(Rp,S)-COP-OAc]2 in dichloromethane
T=23°C; Inert atmosphere;
参考文献
Cannon, Jeffrey S.; Kirsch, Stefan F.; Overman, Larry E.
Journal of the American Chemical Society, 2010 , vol. 132, # 43 p. 15185 - 15191
反应条件
palladium-barium carbonate; Petroleum ether
Hydrogenation;
参考文献
Hennion et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1142
参考文献
Young; Webb
Journal of the American Chemical Society, 1951 , vol. 73, p. 780
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Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1949 , p. 623,627136,138
Chem.Abstr., 1950 , p. 3920
反应条件
acetic acid
T=25°C; dann bei 50-60grad;
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
反应条件
acetic acid
T=25°C; dann bei 50-60grad;
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
反应条件
1: hydrogen chloride / 0 °C
2: NaHCO3 / 45 °C
3: hydrogen chloride / 0 °C
4: glacial acetic acid / 25 °C / dann bei 50-60grad
View Scheme
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
反应条件
1: phosphoric acid
2: palladium/barium carbonate; petroleum ether / Hydrogenation
View Scheme
参考文献
Hennion et al.
Journal of Organic Chemistry, 1956 , vol. 21, p. 1142
反应条件
1: NaHCO3 / 45 °C
2: hydrogen chloride / 0 °C
3: glacial acetic acid / 25 °C / dann bei 50-60grad
View Scheme
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
反应条件
1: NaHCO3 / >50
2: hydrogen chloride / 0 °C
3: NaHCO3 / 50 °C
4: hydrogen chloride / 0 °C
5: glacial acetic acid / 25 °C / dann bei 50-60grad
View Scheme
参考文献
Nasarow; Aserbajew
Zhurnal Obshchei Khimii, 1948 , vol. 18, p. 419,421
Chem.Abstr., 1949 , p. 114
反应条件
aluminum oxide; di-isopropyl ether; silica gel; thorium(IV) dioxide
参考文献
Eastman Kodak Co.
Patent: US2685598 , 1951 ;
