1,1-二甲基-2-丙烯基乙酸酯合成路线 （共 69 条）
反应条件
lt;Mo(CO)4Br2gt;2 in dichloromethane
2 h; Ambient temperature; Yield given;
参考文献
Malkov, Andrei V.; Davis, Stuart L.; Baxendale, Ian R.; Mitchell, William L.; Kocovsky, Pavel
Journal of Organic Chemistry, 1999 , vol. 64, # 8 p. 2751 - 2764
反应条件
indium trifluoromethanesulfonate in dichloromethane
T=25°C; Friedel Crafts reaction; 2 h;
参考文献
Vece, Vito; Ricci, Jeremy; Poulain-Martini, Sophie; Nava, Paola; Carissan, Yannick; Humbel, Stephane; Dunach, Elisabet
European Journal of Organic Chemistry, 2010 , # 32 p. 6239 - 6248
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 273,277
Chem.Abstr., 1952 , p. 882
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1951 , p. 273,277
Chem.Abstr., 1952 , p. 882
反应条件
phenate de sodium phenylphosphinate d'isopropyle; niobium bromide in N,N-dimethyl-formamide
T=100°C;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 383 - 408
反应条件
triphenylphosphine-3,3',3''-trisulfonic acid trisodium salt; (EMIM) tetrafluoroborate; palladium diacetate in water
Tsuji-Trost reaction; microwave irradiation;
参考文献
Liao, Meng-Chun; Duan, Xin-Hua; Liang, Yong-Min
Tetrahedron Letters, 2005 , vol. 46, # 20 p. 3469 - 3472
反应条件
sodium hydride; bis-diphenylphosphinoethane; Pd(1,2-bis(diphenylphosphino)ethane)2 in tetrahydrofuran
36 h; Heating;
参考文献
Cuvigny, Therese; Julia, Marc; Rolando, C.
Journal of Organometallic Chemistry, 1985 , vol. 285, p. 395 - 414
反应条件
Cl2Ni(1,2-bis(diphenylphosphino)ethane) in tetrahydrofuran
T=65°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. C21 - C24
反应条件
1: 41 percent / CoCl2DPPE, NaBH4 / dimethylformamide / 100 °C
2: NiCl2DPPE, i-PrMgCl / tetrahydrofuran / 36 h / Heating
View Scheme
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1983 , vol. 250, # 1 p. C21 - C24
反应条件
methylmagnesium bromide; sodium hydride; NiCl2((PPh3)P)2 in tetrahydrofuran
T=65°C; 36 h; other reag.; other catalyst; other temp./react. time; other solvents; Product distribution;
参考文献
Cuvigny, Therese; Julia, Marc
Journal of Organometallic Chemistry, 1986 , vol. 317, p. 383 - 408
