3,3',5,5'-四叔丁基-4,4'-联苯醌合成路线 (共 172 条)
反应条件
manganese triacetate; acetic anhydride in acetic acid T=100°C; 0.5 h; Further byproducts given;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 2 p. 620 - 622
反应条件
manganese triacetate; ammonium chloride in acetic acid T=100°C; 0.166667 h;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 65, # 2 p. 620 - 622
反应条件
sodium methylate in methanol Ambient temperatureelectrolysis; anode: glassy carbon plate; cathode: platinum foil; S.C.E.; 0.5 V; 0.1 M NaClO4;
参考文献
Chemical & Pharmaceutical Bulletin, , vol. 33, # 9 p. 4007 - 4011
反应条件
potassium tert-butylate in N,N-dimethyl-formamide; Petroleum ether; benzene T=-78 - -60°C; 1 h; Further byproducts given;
参考文献
Journal of Organic Chemistry, , vol. 48, # 21 p. 3700 - 3703
反应条件
manganese(IV) oxide in benzene T=0 - 10°C; 2.5 h;
参考文献
Journal of Organic Chemistry, , vol. 48, # 21 p. 3700 - 3703
反应条件
manganese(IV) oxide in chloroform 1 h; Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 40, # 6 p. 1452 - 1461
反应条件
potassium tert-butylate in tert-butyl alcohol 120 h; Yields of byproduct given;
参考文献
Liebigs Annales, , # 7 p. 1183 - 1186
反应条件
potassium tert-butylate in tert-butyl alcohol 96 h; Ambient temperature;
参考文献
Liebigs Annales, , # 7 p. 1183 - 1186
反应条件
1: 89.4 percent / 5.0 molpercent Pd(PPh3)4 / tetrahydrofuran / 3 h / Ambient temperature 2: 96.1 percent / tetrabutylammonium fluoride / tetrahydrofuran / 0.02 h / Ambient temperature 3: K3Fe(CN)6, KOH / benzene / 51 h / Ambient temperature View Scheme
参考文献
Heterocycles, , vol. 43, # 5 p. 941 - 944
反应条件
lead dioxide; trifluoroacetic acid in water T=33 - 38°C;
参考文献
Journal of Organic Chemistry, , vol. 73, # 3 p. 858 - 867