2-羟基-3-氯丙基乙酸酯合成路线 （共 16 条）
反应条件
sodium acetate; iron(III) chloride in dichloromethane; acetic acid
参考文献
The United States of America as represented by the Secretary of the Navy
Patent: US4395561 A1, 1983 ;
反应条件
anhydrous iron chloride T=20 - 70°C; 24.1667 h;
参考文献
Bristol-Myers Squibb Company
Patent: US2008/9465 A1, 2008 ;
Location in patent: Page/Page column 81 ;
US 20080009465 A1
反应条件
Sn-P in benzene 20 h; Heating; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Bukowska, Agnieszka; Bukowski, Wiktor
Organic Process Research and Development, 2002 , vol. 6, # 3 p. 234 - 237
反应条件
potassium carbonate 1 h; Reflux; chemoselective reaction;
参考文献
Mallesha; Rao, S. Prahlada; Suhas; Gowda, D. Channe
Journal of Chemical Research, 2011 , vol. 35, # 9 p. 536 - 539
反应条件
pyridine in diethyl ether Ambient temperature;
参考文献
Fujiwara, Masahiro; Hitomi, Kazuhisa; Baba, Akio; Matsuda, Haruo
Synthesis, 1990 , # 2 p. 106 - 109
反应条件
hydrogenchloride T=100°C; 23.75 h; Product distribution / selectivity;
参考文献
DOW GLOBAL TECHNOLOGIES INC.
Patent: WO2006/20234 A1, 2006 ;
Location in patent: Page/Page column 33-37 ;
反应条件
1,3-dichloro-1,1,3,3-tetrabutyldistannoxane T=50°C; Acetylation; 5 h;
参考文献
Orita, Akihiro; Ito, Toshihide; Yasui, Yutaka; Otera, Junzo
Synlett, 1999 , # 12 p. 1927 - 1929
反应条件
1,3-dichloro-1,1,3,3-tetrabutyldistannoxane T=40°C; Acetylation; 50 h;
参考文献
Orita, Akihiro; Ito, Toshihide; Yasui, Yutaka; Otera, Junzo
Synlett, 1999 , # 12 p. 1927 - 1929
反应条件
iron(III) chloride Ring cleavage;
参考文献
Ogawa, Hiroshi; Kodera, Yasutake; Kanoh, Shigeyoshi; Ueyama, Akihiko; Motoi, Masatoshi
Bulletin of the Chemical Society of Japan, 1998 , vol. 71, # 2 p. 433 - 442
参考文献
Mattocks,A.R.
Journal of the Chemical Society, 1964 , p. 4840 - 4845
