1,1,1,5-四氯戊烷合成路线 （共 31 条）
反应条件
tetrachloromethane T=40°C; Rate constant;
参考文献
Gasanov, R. G.; Ivanova, L. V.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 5 p. 895 - 899
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 5 p. 1011 - 1015
反应条件
decacarbonyldimanganese (2); isopropyl alcohol T=120°C; 2 h; other reagents, reagents ratios; Product distribution;
参考文献
Moskalenko, M. A.; Terent'ev, A. B.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 3 p. 479 - 482
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 3 p. 637 - 641
反应条件
hexacarbonyl chromium T=120°C; relative rate of telomerization initiated by Cr(CO)6 and further initiator; partial chain-transfer constants; Product distribution;
参考文献
Grigor'ev, N. A.; Tumanskaya, A. L.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1982 , vol. 31, # 1 p. 187 - 190
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1982 , # 1 p. 199 - 202
反应条件
dibenzoyl peroxide T=90°C; 3 h; variation of the reactant ratio; Product distribution;
参考文献
Grigor'ev, N. A.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 3 p. 443 - 447
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 3 p. 625 - 629
反应条件
T=39.9°C; Rate constant;
参考文献
Il'inskaya, L. V.; Gasanov, R. G.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1988 , vol. 37, # 6 p. 1236 - 1238
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1988 , # 6 p. 1402 - 1404
反应条件
1: ethanolic ammonia / beim anschliessenden Behandeln mit Wasserstoff in Gegenwart von Platin 2: zinc; ethanol 3: palladium/barium sulfate; methanol. ammonia / Hydrogenation 4: sodium iodide; 2-ethoxy-ethanol View Scheme
参考文献
Nesmejanow et al.
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1955 , p. 657,660;engl.Ausg.S.585,587
反应条件
hexacarbonyl molybdenum in chloroform T=140°C; 5 h; other catalyst, solvent; Product distribution;
参考文献
Kuz'mina, N. A.; Blinova, N. V.; Chukovskaya, E. Ts.; Grechkina, E. M.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1986 , vol. 35, # 5 p. 1032 - 1036
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1986 , # 5 p. 1139 - 1142
反应条件
decacarbonyldimanganese (2); butane-1-thiol T=140°C; 4 h;
参考文献
Petrova, R. G.; Churkina, T. D.; Golikova, I. A.; Freidlina, R. Kh.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1983 , vol. 32, # 8 p. 1642 - 1646
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1983 , # 8 p. 1816 - 1820
参考文献
du Pont de Nemours and Co.
Patent: US2398430 , 1942 ;
Full Text Show Details
du Pont de Nemours and Co.
Patent: US2410541 , 1942 ;
反应条件
anhydrous tetramethylammonium chloride in methanol; water (electrochemical reduction);
参考文献
Nagao,M. et al.
Journal of the American Chemical Society, 1966 , vol. 88, p. 3447 - 3449
