1,1-双(三甲基硅氧基)乙烯合成路线 （共 5 条）
反应条件
phenanthrene in tetrahydrofuran; diethyl ether
T=-78°C; also at other temperatures, various reaction times; Product distributionMechanism;
参考文献
Bellassoued, Moncef; Gaudemar, Marcel
Tetrahedron Letters, 1990 , vol. 31, # 2 p. 209 - 212
反应条件
sodium hexamethyldisilazane
1) ether, -78 deg C, 1.5 h, 2) room temperature, 12 h; Multistep reaction. Title compound not separated from byproducts;
参考文献
Sergeev, V. N.; Baukov, Yu. I.
J. Gen. Chem. USSR (Engl. Transl.), 1980 , vol. 50, # 5 p. 1059 - 1064,851 - 855
反应条件
(i) LDA, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Ainsworth,C.; Kuo,Y.-N.
Journal of Organometallic Chemistry, 1972 , vol. 46, p. 73 - 87
参考文献
Rudakova,T.A. et al.
J. Gen. Chem. USSR (Engl. Transl.), 1969 , vol. 39, p. 2026 - 2031,1982 - 1985
反应条件
(i) LDA, (ii) /BRN= 1209232/; Multistep reaction;
参考文献
Kuo,Y.-N. et al.
Journal of the Chemical Society [Section] D: Chemical Communications, 1971 , p. 136 - 137
