反应条件
1: sodium borohydride, calcium chloride / methanol / 1 h / 0 °C 2: 68.68 percent / pyridine / CHCl3 / 24 h / Ambient temperature 3: 1.) palladium acetate, triphenylphosphine, 2.) Dibal-H / 1.) xylene, reflux, 24 h, 2.) ether, -50 deg C, 30 min, 20 deg C, 30 min, 45 deg C, 30 min View Scheme
参考文献
Indian Journal of Chemistry - Section B Organic and Medicinal Chemistry, , vol. 35, # 6 p. 530 - 533
